GCMS analysis sample AD26537, non-target compounds, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File c: \HPCHEM\1\DATA\DEC0701\26537 .D Vial: 4 Acq On 7 Dec 2001 8:51 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxepane, 2,2,4-trimethyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.14 5.44 ng/uL 1451540 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxepane, 2,2,4-trimethyl- 100 C6H120 023120-44-7 38 2 l-Hexene / 84 C6H12 000592-41-6 23 3 Pentane/ 2,3-dimethyl- 100 C7H16 000565-59-3 16 4 Oxirane, tetramethyl - 100 C6H120 005076-20-0 14 Abundance Scan 32 (5.136 min): 26537.D (-) m/z 4 ..10 100.00% 41 56

5000 71 5.00 5.20 5.40_______ + 100

K 47 51 । 61 mmmmp |l‘"l>l'l|lll‘l" 1111111111.. |.... | >. l rf-rrtr-fTupn, m/ z 56.10 72.50% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1525: Oxepane, 2,2,4-trimethyl- 43 59

5000 ■ • । * ■ • • i • » —If 5.00 5.20 5.40_______ m/z 5 1.10 70.46% 31 85 i ! 1 { 1 1 ! TIT >100 TWumag . | . j ■ , Tut TITTTO—nuaTTTT Hmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 05 100 105 110 miz-> Abundance #62755:1 -Hexene 41 56 27 • • ) • • T 5.00 5.20 5.40______

A 5000 m/z 42.10 70.02% 84 69

miz-> TIUTHIUTTT TII—09Ba01 5tL 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #1597: Pentane, 2,3-dimethyl- 43 55 5.00 5.20 5.40______ m/z 43.10 68.80% 5000 27 71

miz—> ■ ■ i1 ■ ■ ■ r I ‘‘ ‘ I' ‘' I m 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 85 too - 5.00 5.20 5.40 TFTi

26537.D NP112701.M Thu Dec 13 11:27:13 2001 Page 3

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