Laboratory report documenting GCMS analysis of sample AD26677 identifying unknown compounds on December 10, 2001.
NYC-WTC_000031989–000032006Folder label: “GCMS X 11/7/01 A 12/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC0 601\26677.D Vial: 11 Acq On 6 Dec 2001 7:17 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 8 Oxepane, 2,2,4-trimethyl- Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
10.32 1.35 ng/uL 379304 1,4-Dichlorobenzene-d4 11.89
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Oxepane, 2,2,4 - trimethyl - 100 C6H120 023120-44-7 23 2 Oxirane, 2,2- imethyl-3-propyl- 114 C7H140 017612-35-0 17 3 Pyrrolidine, -methyl- 85 C5H11N 034375-89-8 14 4 Ether, 3-butenyl propyl 114 C7H140 ________034061-75-1 12 Abundance Scan 597 (10.319 min): 26677.D (-) m/z 43.05 100.00% 43
5000 59
73 85 L 1 I'I ।‘| । । । ।100f । > > । । । । । । । । | ' ' i' ■ ' 1 i 1 _J 10.00 1 0.20 10.40 10.60 m/z 59.10 46.46% 'm/z—> 10 20 30 40 50 60 70 80 90 100 110 120 'Abundance #1525: Oxepane, 2,2,4-trimethyl- 43 59
5000- ' ' I ’ • -rfr f ' ' ' I 10.00 10.20 10.40 10.60 m/z 55.10 43.78% i m/z~> . . । . . . . । . 10 20 31 ■ I*- ■ ■ • I 30 40 4ll 50 60 85 1 _ _ ' I 1 ' 1 ' I ' 1 ' ’ i 1 70 80 90 100 100 110 120 Abundance #3003; Oxirane, 2,2-dimethyl-3-propyl- 43 59 85 10.00 10.20 10 40 10.60 5000- m/z 57.10 35.30% 72 , ■ , | 99 114 . ' 1 i ' ' ' ' i ' — ——— TPTT —IIP TPF-PITT miz- 10 20 30 40____ 50 60 70 80 90 100 110 120 Abundance #637: Pyrrolidine, 3-methyl- TAm-T ' TITNTT i 43 10.00 10.20 10.40 10.60 m/z 41.10 34.46% 5000
85 15 27
miz-> -- 10 20 30 40 — ——— 50 56
60 68
70 -..................... .. ' 80 90 100 110 120 ---A PT 10.00 10.20 10.40 10.60
26677.D NP112701.M Fri Dec 07 14:52:33 2001 Page 8
NYC-WTC_000032003
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NYC-WTC_000031968
Laboratory report documenting GCMS analysis of sample AD26676 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032245
Gas chromatography-mass spectrometry analysis of sample AD26832 documenting unknown compounds with reference to comments.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032007
Laboratory report documenting GCMS analysis of sample AD26678 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032142
Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 5, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032202
Laboratory report documenting GCMS analysis of sample AD26829 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032093
Laboratory report documenting GCMS analysis of sample AD26682 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031920
Laboratory report documenting GCMS analysis of sample AD26625 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032058
Laboratory report documenting GCMS analysis of sample AD26680 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032343
Laboratory report for GCMS analysis of sample AD26982 completed on December 11, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032182
Laboratory report documenting GCMS analysis of sample AD26828 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031333
Laboratory report documenting GCMS analysis of sample AD26321 with unidentified compounds detected.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032362
Laboratory report for GCMS analysis of sample AD26983 completed on December 11, 2001, with surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000031869
Illegible text on a single page from the GCMS folder covering November to December 2001.
Filed in the same folder
NYC-WTC_000031870
Index or cover sheet page for the GCMS folder covering the period from November 7 to December 6, 2001.
Filed in the same folder
NYC-WTC_000031876
Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.
Filed in the same folder
NYC-WTC_000031889
GC/MS analysis of sample AD26538 identified other unknown compounds noted in comments section, December 10, 2001.
Filed in the same folder
NYC-WTC_000031905
Laboratory report documenting GCMS analysis of sample AD26624 identifying unknown compounds on December 10, 2001.
Filed in the same folder