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GCMS Analysis Report for Sample AD26389, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26389 with a note regarding unknown compounds.

NYC-WTC_000031473–000031490

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26389.D Vial: 6 Acq On : 30 Nov 2001 4:46 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1,4-Dichlorobenzene-d4 Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 11.74 0.54 ng/uL 229246 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlor enzene-d4 150 C6C12D4 003855-82-1 94 2 Benzene-1, ,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 42 3 Benzalde: de, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 9 4 2H-1-Be: opyran-3-ol, 3,4-dihydro- 150 C9H10O2 021834-60-6 9 Abundance Scan 753 (11.745 min): 26389.D (-) m/z 150.00 100.00% 150

5000 115 52 78 87 1140 11‘so 1180 IZOD “ 1 ' miz-> 1 ■ । ■ 30 —HHP 40

40 50 . 62

60 — IIPP 70 80 90 100 11C • ■ i ■ ■ ■' i ■' 130 140 I— m/z 152.00 150 160 64.82% Abundance #9593: 1,4-Dichlorobenzene-d4 150

5000 115 i — j ----- P

78 11.40 11.60 11.80 12.00 52 m/z 115.05 , 44.95% 35 87 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ 11111111 ।।.।. P ' 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■' —— miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 -Prr,1 115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 26.50%

35 87 I - L ■11'' •' i1 ‘ • i -n-p-r-n-p-r T_................ ’t111 , r-n-p-r miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 11.40 11.60 11.80 12.00 m/z 52.00 23.12% 106 5000 53 81

122 । ‘‘1‘+11111131 -n-p-r-n-p-r 92 ...... 1....... 136........ | 11‘ III IT 1 * 1 1 * i'' ‘ ‘ i 1 •' ‘ i ‘ ‘ ‘ ‘ i ' • ‘ ‘ i 1 ' i • ---T m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

26389.D NP112701.M Tue Dec 04 10:41:09 2001 Page 9

NYC-WTC_000031489

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NYC-WTC_000031489Source: NYC Law Department, mirrored locally

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