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GCMS Analysis Report for Sample AD26389, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26389 with a note regarding unknown compounds.

NYC-WTC_000031473–000031490

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ? C:\HPCHEM\1\DATA\NOV3001\26389.D Vial? 6 Acq On ? 30 Nov 2001 4:46 pm Operator? GALOS Sample ? gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr? 1.00 MS Integration Params? LSCINT.P Quant Method ? C? \HPCHEM\1\METHODS\NP112701 .M (RTE Integrator) Title ? 208 625/TCLP calibration table Library ? C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Hexane, 2-methyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 10.53 0.67 ng/uL 285903 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

l Hexane, 2 -mi thyl- 100 C7H16 000591-76-4 27 2 2 -Hexanone 3,3-dimethyl- 128 C8H160 026118-38-7 25 3 Pentanal,2,2-dimethy1- 114 C7H140 014250-88-5 25 4 Nonane <5-methyl- 142 C10H22 015869-85-9 17 Abundance Scan 621 (10.534 min): 26389.D (-) m/z 43.10 100.00% 43

5000

mpmmmmmmmm m + 4 57 85

100 5l.+ li J >■ >i !■ J(> ■ ■ >( ■ ■ >t r rrti TMp 1 10.20 10.40 10.60 10.80 m/z 45.00 JU 43.79% miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63433: Hexane, 2-methyl- 43

5000 —A T T 10.20 10.40 10.60 10.80 T

27 57 85 m/z 41.10 26.26%

m/z-> 5 | । ■ 11111111 j > TTT i hi 11... ।... I! 11.... ।.... | 71 . 100 .. ।.... |.... 11... ।.... ।... t i... |. u i j i... |, TE 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 l Abundance

5000 #5126: 2-Hexanone, 3,3-dimethyl- 43 frTr Lu A 10.20 10.40 10.60 10.80 m/z 85.05 24.18% 85

m/z—> Abundance ___ 15 27 _____ . ■ 11 ■ 111111 n TT TTmpgmmbgTmmmi 1’1 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #3038: Pentanal, 2,2-dimethyl- 43 57 69____ 1 T a 10.20 10.40 10.60 10.80 m/z 57.10 17.51% T

5000 85 27 57 72

m/z-> -AH m TU X 5 10 15 20 25 3035404550556065 70 75 80859095 100105 1 > ] 1 ■ | ■ 1111111 n ■ | , — —A ■ । m . . I 10.20 10.40 10.60 10.80

26389.D NP112701.M Tue Dec 04 10:41:08 2 001 Page 8

NYC-WTC_000031488

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NYC-WTC_000031488Source: NYC Law Department, mirrored locally

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