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GCMS Analysis Report for Sample AD26389, Dec 2001

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Report documenting GCMS analysis of sample AD26389 with a note regarding unknown compounds.

NYC-WTC_000031473–000031490

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26389.D Vial: 6 Acq On : 30 NOV 2001 4:46 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexane, 2-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 10.32 1.54 ng/uL 656622 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

l Hexane, /2- me thy 1- 100 C7H16 000591-76-4 35 2 Tetrahydrofuran, 2,2-dimethyl- 100 C6H120 001003-17-4 33 3 Hexane, 2-methyl- 100 C7H16 000591-76-4 25 4 Oxipane, 2,2-dimethyl-3-propyl- 114 C7H140 017612-35-0 20 Abundance Scan 598 (10.323 min): 26389.D (-) m/z 43.05 100.00% 43

5000- ___ 57 85 fTer 10.00 10.20 10.40 10.60 73

miz-> 3 1 454— mHlm Np m/z 89 100 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 57.10 29.07% Abundance #63434: Hexane, 2-methyl- 43

5000- — AA 10,00 10,20 10.40 10.60 ‘I 57 85 m/z41.1026.08% 29

mlz-> Lm .............. . ............ 69................. , 100 11"1 • i' ■'' 1 1,1111,11111111''111 • ■ ■ ■ i ■ ■'1 .... I.... I.... I..■> I.... I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63380: Tetrahydrofuran, 2,2-dimethyl- 43 PTT 10.00 10.20 10.40 10.60 5000 m/ Z 85.0,5 23.90% 85 59

27,31 +534 70 I > i [ > a > >| ■ I ■ I'l 11111 >r> 111 Ppaam I.., p.।. p-rr. ।.... | miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63433: Hexane, 2-methyl- T — T T 43 10.00 10.20 10.40 10.60 m/z 59.10 23.33% 5000-

57 85 27 71 100 miz—> mmmmm 11'' ■ • i ■ ‘‘ I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 111 ■' ‘ ‘ i' “ ■ i1'' * i ‘ ‘ • i' ‘ ‘1 10——— TOI I I 1 1 I I I 10.00 10.20 10.40 10.60

26389.D NP112701.M Tue Dec 04 10:41:07 2001 Page 7

NYC-WTC_000031487

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NYC-WTC_000031487Source: NYC Law Department, mirrored locally

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