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GCMS analysis result with unknowns, Dec 2001

Machine-extracted title · confidence 100%

Analysis report for sample AD26391 indicating the presence of other unknown compounds on December 4, 2001.

NYC-WTC_000031509–000031529

Folder label: “GCMS X 11/5/01 A 12/1/01

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Scanned page image, NYC-WTC_000031528
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26391.D vial: 7 Acq On : 30 Nov 2001 5:41 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1,4-Dichlorobenzene-d4 Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 11.74 0.54 ng/uL 252853 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Te: ative ID MW MolForm CAS# Qual

1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene-1,2, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 2H-1-Benzopyran-3-ol, 3,4-dihydro- 150 C9H10O2 021834-60-6 9 4 Benzoic-acid, 2,5-dimethyl-150 C9H10O2 000610-72-0 9 Abundance Scan 753 (11.744 min): 26391 .D (-) m/z 150.00 ,100.00% 150

5000 115 52 78 40 11.40 11.60 11.80 12.00 87 .63....,1. ■ ।. r’ miz-> 30 -PH 40 50 + 1‘ ’ ‘ 1 1 •’ e —me 1 • i * • • • । * < • > ।' > 60 70 80 90 100 110 120 130 140 150 160 m/z 152.00 62.90% Abundance #9593: 1,4-Dichlorobenzene-d4 150

115 ------- — --------- 5000 78 11.40 11.60 11.80 12.00 52 m/z 115.05 44.89% 35 87 ।। • i ■ 11 ■ > i • • •»1 *1 TTTImgT 1 • i'' • ■ i1' ■' i ■ ■ 1111 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 V 115 11.40 11*60 11.80 12.00 ' 5000 52 78 m/z 78.05 24.67%

miz-> Abundance 30 35 ....... I............. 40 50 60" 70 ' 80 87 _............ i1 111 1 11 1 ' I ' ' 90 100 110 120 130 #9708: 2H-1-Benzopyran-3-ol, 3,4-dihydro- + 140 150 160 - T !T 107 150 11.40 11.60 11.80 12.00 m/z 52.00 , 24.33%

5000 78 119 131

■ ' i1 ‘1' I • ■ ■ ‘ i • ' ‘ 1 I'' ‘ ' i ' 1 , 89 I ' ' ■ ''i • ' • ' i ' ‘ 11 ‘ 5) h I * • * ■ i ■ 11 11 ■ > • । • m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1140 11.60 11.80 12.00 '

26391.D NP112701.M Tue Dec 04 10:42:32 2001 Page 12

NYC-WTC_000031528

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NYC-WTC_000031528Source: NYC Law Department, mirrored locally

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