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GCMS Analysis Report for Sample AD26386, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26386 with a note regarding unknown compounds.

NYC-WTC_000031415–000031432

Folder label: “GCMS X 11/5/01 A 12/1/01

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Scanned page image, NYC-WTC_000031431
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26386.D vial: 12 Acq On : 30 Nov 2001 10:13 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1,4-Dichlorobenzene-d4 Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 11.74 0.55 ng/uL 244101 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene-1,2,3, 4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzoic acid, 2,3-dimethyl- 150 C9H10O2 000603-79-2 9 4 4-Amino-2-chlorobenzonitrile 152 C7H5C1N21 020925-27-3 9 Abundance Scan 753 (11.744 min): 26386.D (-) m/z 150.00 100.00% 150

5000 115 — . i r i i |-r 52 78 11.40 11.60 11.80 12.00 T’uH t ++ ■ — 87 PPP — 1 ‘ 8‘ m/z 152.00 63.19% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 110

115 ----- 5000 78 11.40 11.60 11,80 12.00 52 m/z 115.05 42.86% 35 87 111 ■ ■ ■' |i 111111 I '1 i'''' i11 111111'111111 ‘ 11 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichIoro- 150 * » I * » < i | > * — r i' P

115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 23.30%

35 87 ....... 1, I 111111111111111 ■' i1 ■ ■ ■ i' ■ i ’ ■ ■ ' 1 1 ' ■ ■ i ' ' miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9716: Benzoic acid, 2,3-dimethyl- - 105 132 150 11.40 11.60 11.80 12.00 m/z 52.00 . 22.42% 77 5000 51

63 ............................. |......... I i 11111 — 11 — / I - ‘ ‘ I ‘ ' I ‘ ‘ ‘ I * ‘ 1 ‘ 11 ‘ ‘ ‘ I ‘ ‘ । ■111 ■ ■ ■ ■ । ‘ i ■ •'11 1 ■ I' ■ ‘11′1117 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

26386.D NP112701.M Tue Dec 04 10:38:38 2001 Page 9

NYC-WTC_000031431

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NYC-WTC_000031431Source: NYC Law Department, mirrored locally

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