NYC-WTC_000032591
Laboratory report for GCMS analysis of sample AD27013 completed on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GCMS method 208 data table, Dec 2001
Machine-extracted title · confidence 90%Data table containing pH and volume measurements associated with GCMS method 208 analysis procedures.
NYC-WTC_000031213–000031222Folder label: “GCMS X 11/3/01 A 12/1/01”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\LB.D Vial: 2 Acq On : 30 Nov 2001 1:08 pm Operator: GALOS Sample : 1b 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.74 0.52 ng/uL 248822 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene-1, 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzol/c acid, 2,5-dimethyl- 150 C9H10O2 000610-72-0 9 4 Benzoic acid, 2,3-dimethyl- 150 C9H10O2 000603-79-2 9 Abundance Scan 752 (11.741 min): LB.D (-) m/z 150.00 100.00% 150
5000 115 —i----- 52 78 40 11.40 11.60 11.80 12.00 TIIr -H H 63 I ‘ ‘ ‘ I ’1 87 i ■ ‘ • • i''' ■ i ■ ■ ‘I ' । ■ ■ ■ 111 ‘ । ■ i |, I • TT m/z 152.00 63.33% mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593: 1,4-Dichlorobenzene-d4 150
- 5000 115 78 11.40 11.60 11.80 12.00 52 m/z 115.05 , 43.04% 35 87 L ‘III 11 I ‘ 1 ‘1 I ‘ ‘ ‘ ‘ I r-r-p-T-n-p-T ! ' T’ r • rT rj . I I • I 11 ——mm—B—Ipur m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150
115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 24.42%
35 87 |_____ ■ ' i ■ ■ ‘ ‘ i ■ ' ‘ ' I ‘ 11111113 _......... , . 1. < • • l • • 1 ' I ' “ 1 I ' 1 " I " I > 11 H । 1 —I miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 • ‘i 11 >1 । _ . 4. rri — Abundance #9719: Benzoic acid, 2,5-dimethyl- 104 132 150 11.40 11.60 11.80 12.00 m/z 52.00 23.32%
5000 77 51 66 I । /1 — | i i — r
m/z—> IPI —30 11- 40 50 60 70 80 90 I ' TIIt' —11a 100 110 120 130 140 150 160 “ I ' ■ ' ■ I ‘ ‘ 11.40 11.60 11.80 12.00
LB.D NP112701.M Tue Dec 04 10:13:49 2001 Page 3
NYC-WTC_000031221
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NYC-WTC_000031221Source: NYC Law Department, mirrored locally
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Calibration data sheet for GCMS analysis using TCLP method, listing standards and response factors from December 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
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Calibration data table for gas chromatography-mass spectrometry analysis dated December 3, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
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Calibration data sheet for GCMS analysis using TCLP method, listing standards and response factors from December 2001.
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Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
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Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Filed elsewhere
NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
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Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · similarity 0.993
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DEP laboratory report documenting GC/MS results for sample AD25830 analyzed on December 6, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035518
Calibration data sheet for GC/MS analysis dated December 28, 2001, listing deuterated standards.
1 shared topics · similarity 0.992
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NYC-WTC_000031415
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031602
DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26471 noting other unknown compounds.
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