GCMS comments for sample AD26473 detecting N,N-dimethylbenzenesulfonamide

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26473.D Vial: 9 Acq On : 30 Nov 2001 7:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 l,4-Dichlorobenzene-d4 Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 11.74 0.50 ng/uL 207860 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene-l,/,3,4-d4-, 5,6-dichioro- 150 C6C12D4 002199-69-1 42 3 Benzoic acid, 2,5-dimethyl- 150 C9H10O2 000610-72-0 9 4 ((3-Etho: henyl)-1-methanol_____ 152 C9H1202 000000-00-0 9 Abundance 7 Scan 753 (11.745 min): 26473.D (-) m/z 150.00 100.00% 150

5000 115 52 78 ----- -

‘ ■ i ■ 40 -HP I । H IT 63 3.187 4m 11.40 11.60 11.80 12.00 m/z 152.00 63.19% mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593: 1,4-Dichlorobenzene-d4 150

5000 115 7 1 rrp-1 M | M rr j ′ । n । • • « * j • 78 11.40 11.60 11.80 12.00 52 m/z 115.05 , 39.97% 35 111 ■ ■ ■ ■ I ■ ■ ■11 1’11112111 i ■ ■ ■ ■ i' ■ ■ ■ i ■ ■ ■ ■ i ■ ■1' i ■1 ■11 ■' ■ ■ i • ■ 1 TIIt miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichloro- 150 — P—— 115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 25.44%

35 87 I 1 - ■ ■ i ■1 " i ■1' ■ i ।11 •■।1■•11j1■■i11 T— 1 TITT TTTT m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9719: Benzoic acid, 2,5-dimethyl- V 104 132 150 11.40 11.60 11.80 12.00 " ' ‘ m/z 52.10 22.83% 5000 77 51 66 _................... —...............

miz—> —ImPP 1’4111’11111 I I I I II I I I ( I T I ’1111/1 30 40 50 60 70 80 90 100 110 120 130 140 150 160 TTTT L 11.40 11.60 11.80 12.00

26473.D NP112701.M Tue Dec 04 10:45:13 2001 Page 3

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