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GCMS comments for sample AD26473 detecting N,N-dimethylbenzenesulfonamide

Machine-extracted title · confidence 100%

DEP lab report dated December 10, 2001, identifying N,N-dimethylbenzenesulfonamide at 0.49 ug/L in sample AD26473.

NYC-WTC_000031636–000031649

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26473 .D Vial: 9 Acq On : 30 NOV 2001 7:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butane, 2-ethoxy- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.56 4.90 ng/uL 2558530 Acenaphthene-dl0 20.78 Hit# of 5/ Tentative ID MW MolForm CAS# Qual 1 Butane/ 2-ethoxy- 102 C6H140 002679-87-0 0 2 Butane, 2-ethoxy- 102 C6H140 002679-87-0 47 3 Ethanol, 2-[2-(2-ethoxyethoxy)ethox 178 C8H18O4 000112-50-5 39 4 Ethane, 1,11-oxybis[2-ethoxy-] 162 C8H18O3 000112-36-7 38 Abundance Scan 1932 (22.556 min): 28473.D (-) m/z 45.10 100.00% 45

73 5000 59 _ ----I —T II t t r T 87 103 117

miz-> m hmmmt u J -4 133 147 161 177 m/z l < 1 [ 1 ) ‘I TTTIII0TE111‘11T | i ., , | ..I , H I 11 I I , | . I b I | I I I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 22.20 22.40 22 60 22.80 73.05 54.49% Abundance #1768: Butane, 2-ethoxy- 45

73 ---------- 5000 22.20 22.40 22.60 22.80 27 m/z 72.0,5 42.01% 59 15 ..... | I 102 87 10 25"5b"28-88"88" ‘ 1′1111 70* ‘ 80 "'96'18578 *120 738 140 150 160 170 180 ‘ nlz-> Abundance #63539: Butane, 2-ethoxy- 45 T T8 22.20 22.40 22.60 22.80 73 m/z 59.10 28.50% 5000

59 31 i I ------ . j . i87 102_______________________ : i । . i . i | i . . i । i » : » j : » » . | » » » . | . i i iJ : » i » | U » » j i i : i j . » : miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17075: Ethanol, 2-[2-(2-ethoxyethoxy)ethoxy}- 1 b i ■ ' ■ i ‘ 1 1 45 22.20 2240 22.60 22.80 m/z 43.10 13.66% 5000 59 72 31 । 89

m/z—> T T 1 TTa T" J .. 193 ThTli.TI—tuuur TTT,. .. 119 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 । .t... >(.. >. ।.... ।.... ।.... ।.., II 77 22.40 22.60 7780

26473.D NP112701.M Tue Dec 04 10:45:14 2001 Page 4

NYC-WTC_000031645

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NYC-WTC_000031645Source: NYC Law Department, mirrored locally

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