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Document / 16 pages

GCMS analysis results for sample AD26206, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26206 with unidentified compounds detected.

NYC-WTC_000031171–000031186

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26207.D Vial: 54 Acq On : 30 Nov 2001 6:37 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Ethane, 1,1’-oxybis[2-ethoxy-] Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 22.43 107.95 ug/1 33101500 Acenaphthene-dl0 20.58 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Ethane, 1,1’-oxybis[2-ethoxy-] 162 C8H18O3 000112-36-7 39 2 Ethane, 1,1-diethoxy- 118 C6H14O2 000105-57-7 38 Butane, 2-ethoxy- 102 C6H14O 002679-87-0 38 4 2-Propanol, 1-(1-methylethoxy)- 118 C6H14O2 003944-36-3 33 Abundance Scan 1893 (22.425 min): 26207.D (-) m/z 44.90 100.00% 45 i 73 5000 59 I : I T I ] TT FiT I I I | i T I T I T I 1 89 103 22.00 22.20 22.40 22.60 22.80 U ,i ,1 133 147 161 177 191 251 । । । । । 11 Tr । 1 TT 1111u-—h—0—-11T-11111101111011011131—Ir m/z 73.00 58.44% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #12866: Ethane, 1,1'-oxybis[2-ethoxy-] 45

5000 31 59 72 ( : : 1 1 । I i : 1 j T 11618 t i i | ♦ i i 22.00 22.20 22.40 22.60 22.80 m/z 72.00 44.14% 87 1931 16 ■1 ' 1 1 • i 1' ‘1 i' • ■ 11 ■ 1 ‘ > i ' ■ ‘ ■ i ■ > ■ ‘ i ■ ■ ‘ • I 1 ।1 ‘ ‘ 1 i ■ ‘ 1 ■ i miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #64432: Ethane, 1,1-diethoxy- 45

22.00 2220 22.40 22.60 22.80 73 m/z 59.05 29.17% 5000

27 15 103 I —H ‘111" 61 ■ ■ । ‘ | । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■11111111 i1 ■ ■ ■ । ■ ■' ■ । miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #63540: Butane, 2-ethoxy- 45 22.00 22.20 22.40 22.60 22.80 m/z 43.00 16.09% 73 5000

27 59 87 102 TTTTTTT - ' i ' ■ ■ ■ i ■ • • ■ i ■' ■ i1 ■ ■' i' T‘I11‘1101‘I*IXOI111I1TT — , , I J , — I y — m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 22.00 22.20 22.40 22.60 22.80

26207.D NP112601.M Mon Dec 03 13:11:00 2001 Page 3

NYC-WTC_000031181

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NYC-WTC_000031181Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004149

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.994

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