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GCMS analysis results for sample AD26011, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26011 conducted on December 12, 2001.

NYC-WTC_000030895–000030906

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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Scanned page image, NYC-WTC_000030904
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2001\26011.D Vial : 4 Acq On : 20 Nov 2001 3:31 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\l\METHQDS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Butane, 2-ethoxy- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.40 2.96 ug/1 785256 Acenaphthene-diO 20.60

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-ethoxy- 102 C6H140 002679-87-0 49 2 2-Propanol, 1 -(1-methylethoxy) - 118 C6H14O2 003944-36-3 40 3 Ethane, 1,1 -diethoxy- 118 C6H14O2 000105-57-7 38 4 Ethane, 1,1-oxybis[2-ethoxy-] 162 C8H18O3 ____ 000112-36-7 36 Abundance 7 Scan 1890 (22.397 min): 26011.D (-) m/z 45.0,0 100.00% 45 73 5000 59 89 103 117 22.00 22.20 22.40 22.60 22.80 im/z-> -l h i'1TT - 133 147 161 177 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 111111 TT TT । ii 1111TTT 11111 m/z 73.00 59.46% Abundance #63539: Butane, 2-ethoxy- 45

73 5000 22.00 22.20 22.40 22.60 22.80 59 m/ z 72.0,0 46.00% i 31 , l 87 102 ■ i " " I ■' " i " " i' ' I' ‘ ‘i 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 'Abundance #3549; 2-Propanol, 1-(1-methylethoxy)- 45

22.00 22.20 22.40 22.60 22.80 5000 59 m/z 59.05 29.91%" 31 73 1 ,88 103 ’ ' | 1 ‘ ' 1 | ‘ ' TTTT TIUT " • ’ | • I M IJ | . I I i | I • «I | I ( | . I . ! | i"" i1"' i ■ ■■ > । I ' • ’1 i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 'Abundance #3536: Ethane, 1.1 -diethoxy­ 45 22.00 22.20 22.40 22.60 22.80 m/z 43.00 14 . 77% 5000- 73

27 I 103

miz-> —5.. 1.. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ' * । 6- — P I— — I— 22.00 22.20 22.40 22.60 22.80

26011.D NP103001.M Tue Dec 11 09:22:54 2001 Page 3

NYC-WTC_000030904

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NYC-WTC_000030904Source: NYC Law Department, mirrored locally

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