GCMS analysis results for sample AD26206, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26207.D vial: 54 Acq On : 30 NOV 2001 6:37 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Carbonochloridic acid, methyl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 11.97 5.85 ug/1 .316360 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Carbonochloridic acid, methyl ester 94 C2H3C102l 000079-22-1 42 2 Carbonochloridic acid, ethyl ester 108 C3H5C1O21 000541-41-3 32 3 2-Propanol, 1.1’-oxybis- 134 C6H14O3 000110-98-5 10 4 2-Butanol, 3,31-oxybis- 162 C8H18O3 054305-61-2 10 Abundance 7 Scan 754 (11.969 min): 26207.D (-) m/z 59.0,0 100.00% 59

5000 45 72 1 ‘1/11/1/11/1/1/2.11/8 1tt I TT 1 1 I 1

.... 3944—5051.4 60 4 65 | 79 85 93 101107 116123 HT—uuagTaaemDgTTTpTT 137 11.60 11.80 12.00 12.20 m/z 72.00 47.32%

L ■ i'' miz-> 20 30 40 70 80 90 100 110 120 130 140 Abundance #986: Carbonochloridic acid, methyl ester • 59

5000 TT [ I r i i f * TT I | ’ 1160 11.80 12.00 12.20 55 m/z 44.90 43.98%

miz—> 35 44 -PP — — Th 20 30 40 50 TTT Lx 94 _ 111 60 70 80 90 100 110 120 130 140 Abundance #63749: Carbonochloridic acid, ethyl ester 23 = 63 11.60 11.80 12.00 12.20 5000 m/z 62.95 43.74%

45 35 93 — • • । • • • > । TT 11 T’r i j .... । i i i i । , miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1-oxybis- 59 11.60 11.80 12.00 12.20 1 m/z 43.05 18.18% 31 5000 45

103 — - i i / y — i - 89 72 ■ ■ । ■ ■ ■ ■ । ■ • • ■ । ■1 ■ ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ ■ ‘ । •1 * TUT 'i■ ■1 ■ I' 11 1 i m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.60 11.80 12.00 12.20

26207.D NP112601.M Mon Dec 03 13:10:58 2001 Page 2

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