GCMS unknown compounds report, sample AD31432, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JANI802\31432.D Vial: 10 Acq On : 19 Jan 2002 12:24 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1,1' -oxybis- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.27 0.29 ug/1 79299 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Propanol, 1,1' -oxybis- 134 C6H1403 000110-98-5 56 2 2-Propa: 1-(2-methoxy-1-methylet 148 1, C7H16O3 020324-32-7 50 3 1-Propanol , 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 4 2-Butan'ol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 39 Abundance Scan 678 (11.266 min): 31432.D (-) m/z 59.05 100.00% 69

5000

39. 1 1 45

AU, -4—— 73

84 ■ i’r ■ ■ ■ । ■ । ■ ■ । ■ ■ ■ • । 103

— m/z MN 11.00 11.20 11.40 11.60 45.0, 48.44% m/z-> 30 40I 50 60 70 80 90 100 110 120 130 Abundance #6087: 2-Propanol, 1,1-oxybis- 59 31 5000 45 **1***I*‘*‘1"+‘+I+ 11.00 11.20 11.4Q 11.60 103 m/z 41.00 32.75% 72 89 TIIPIPTPT• I1' im J] i i i > । rl i i । i . . i । . . . . । . m/z-__ 30 40 50 160 70 80 90 100 110 120 130 Abundance -pandl 1-(2-ett ovy 1-ettiyiemor ! 59 AAGAM 11.00 11.20 11.40 11.60 5000 m/z 73.00 30.81%

A 45 103 73 31 I 130 ■ ' i ' 1 ■ ■ i 1 ■ • ■ i ■ • ‘ ■ i ■ ■ ■ ■ i ' ' ‘ i ■ ■ ■ ■ i ' ■ ‘ ■ i ■ 1 ■ • i ■ ■ ■ ' i ' 1 ■ • i ' ■ mtz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086:1-Propanol, 2-(2-hydroxypropoxy)- IIt 59 11.00 11.20 11.40 11.60 m/z 103.0 29.74% 5000 31 45 103

1 1 I 1 1 1 ' I ' 1 ■ ■ i ■ ‘ ,'1 PTr • i ‘ 75■ 1 I ■ ' ■ 89 • i ■ ■ ■ • i ■1 ‘ ■ i ' ■ ■ • i ' ' ' ■ i ■ ■ • . 1*4 1 , . . . . | | . * m/z-> 30 40 50 I60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

31432.D GCMS0103.M Wed Feb 06 15:31:58 2002 Page 3

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