GCMS analysis results for sample AD31465, Feb 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 602\31465.D Vial: 28 Acq On : 17 Jan 2002 3:01 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst* : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, l,l’-oxybis- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.28 0.27 ug/1 77095 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------- 1 1 2 - Propano 1, 1,1’ -oxybis- 134 C6H14O3 000110-98-5 64 2 2-Propanol, 1,1‘-[(1-methyl-1,2-eth 192 C9H20O4 001638-16-0 45 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 42 4 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 39 Abundance Scan 679 (11.276 mln): 31465.D (-) m/z 59.05 100.00% $

45 5000 73 103

miz-> 20 ....... W. 30 40 IT 51 :50 ill 60 ..701 - 80 65.)90......100Y.......... 110 120 m/z 11.00 11.20 11.40 11.60 45.05 52.94% Abundance #6087: 2-Propanol, 1,1-oxybis- 59

31 5000 45 • • i ' 11.00 11.20 11.40 11.60 103 m/z 73.00 1.90% I •14**1 * * I * Y 72 1***/*/*m/*/*1***I**1****11144I18/t 89 m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance *20030 2-Propanol, 1.1(1-methyl-1.2-emanedizlibisoy) 59 ... M... 11.00 11.20 11.40 11.60 5000 m/z 103.05 28.97%

i , m/z-> Abundance 20 31

30 39 40 45

' I • 1 1 ‘ i ■ ■ ■ ■ ! ■ ■ ■ ■ i ■ ■ • ■ i ■ ■ ' 1 i 1 1 1 ' I ' '■’ 1 '| ' 1 11 ( • i i । । । । i । । i । 50 60 59 70 80 73 90 #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 100 103

110 117 120 1IIAAT ----- m/z 4 11.00 11.20 11.40 11.60 41.05 27.57% 5000

m/z—> 20 1 30 40 50 31

।60 45

75 89 103

I ' ■ ■ ‘ i ■ ' ■ ■ i ■ ■ 1 1 I 1 1 ' ' I '

70 80 90 100 1 1 ■ I 1 1 ' ' I ' 110 _ 4 .W — 120 __ _____ 11.00 11.20 11.40 11.60

31465.D GCMS0103.M Thu Feb 07 12:41:30 2002 Page 2

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