GCMS analysis results for sample AD303B5, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30355.D Vial: 7 Acq On : 27 Dec 2001 5:59 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, l,l’-oxybis- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

11.46 0.43 ug/1 112940 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1,1'-oxybis- 134 C6H14O3 000110-98-5 50 2 2-Butanol, 3,3"-oxybis- 162 C8H18O3 054305-61-2 45 3 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 39 4 Silane, ethyldimethyl- 88 C4H12Si 000758-21-4 33 Abundance

5000

39 | 45 Scan 698 (11.456 mln): 30355.D (-) 59

73 103

.84......... 1...................... m/z

M) 59.05 100.00%

11.20 1140 11.60 11.80

M —P+- I ■ ■ " I I'" m/z 45.00 53.56% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087:2-Propanol, 1,1-oxybis- 59

5000 31 45 AA 103 1 11.20 11.40 11.60 11.80 1 m/z 103.00 32.56% 89 । ■ । ■ ■ ■ ■ i ■ ‘ 1 ■ ■ ■ । ■ । itt ■ i721 ■ ■ • i1 ■ ■ ■ i ■ ■ • • i •1 ■ ■ i • ■ ■ ■ i ■ ■ • ■ i ■ ■ ■ • i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3 3‘oxvbis- 59

11.20 11.40 11.60 11.80 m/z 41.0.5 27.28%

N 5000 31 45 103

i ---4 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- AAMAA 59 1 11.20 11*40 11.60 11.80 ‘ m/z 73.00 7.12% 5000 45 103 73 31 +IPPPPPTTH __________ 130 • t ' * • 11' ■ • ■ i 1 ■ 1 ■ i ■ ‘ I * ‘ ’ I ‘ ‘ ‘ I ' 1 ‘ ‘ I ’ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.20 11.40 11.60 11.80

30355.D GCMS1126.M Wed Jan 02 10:55:36 2002 Page 2

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