GCMS analysis results for sample AD303B5, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30355.D Vial: 7 Acq On : 27 Dec 2001 5:59 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.31 0.75 ug/1 238619 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 40 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 4 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9.37 Abundance Scan 1009 (14.311 min): 30355.D (-) m/ z 73.00 100.00% 73

5000 267 355 k ' I ' ‘ • r I ■ ' ‘ TI I I • 1 j . . . 1 | 45 14.00 14.20 14.40 14.60 “ । fi'n I'fiTnJ |Ti i. । 108 133 154 177 193 Tmmmmpt 223 251 323339 1 ‘ | ■ T* , i1] । l i" । । । । i | m/z 266.90 37.55% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 .................... )............................ 5000 1 1 i ■ 1 1 • i’‘i»। i । i i । i i । i । 14.00 14.20 14.40 14.60 m/z 355.0,5 30.70% . | I “ > | .| | ■ i | ■ ■ ■ H > i > 11 i ‘ 191207 251 1 | ‘ । i ( ‘ 1 • ■ | ■ ' • ■ | ■ "1 • | 323339 | | ■ i i ■ i ■ " ■ i' “ • i ■" 'i' “ ‘ i

miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine. N-meth vk beta,. 3 4-tris(trimethyls 73 14.00 14.20 14.40 14.60 5000 355 m/z 267.90 10.37% 44

- 1188 130147 193 267 294 •' ■ । • 11 ■ • 11 ■ ■ - ‘ । • i • ■ । • i ■ • । .।.. ..(.... ( .।■. । ■ , ..|1 .. .।. ,■,। .. .. j m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2,5-bis(trimethylslloxy)-, trimethyls ........ ’I*I*I’+I}+II| 73 14.00 14.20 14.40 14.60 355 m/z 356.0,5 10.24% 5000 45 1 , 147 179 207223 , ’1’13-19001011221209——mTa0100"00TT 267282 370 i ■i 1 I J I I 11. tl l' "I I I1 1] I J—I—I—[ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60

30355.D GCMS1126.M Wed Jan 02 10:55:41 2002 Page 3

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