GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\30313.D Vial: 14 Acq On : 22 Dec 2001 7:31 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.35 0.46 ug/1 130623 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2- (2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 3 2-Propanol, /T, 11 -oxybis- 134 C6H14O3 000110-98-5 50 4 2-Butanol, 1 3,3 ' -oxybis- 162 C8H18O3 0543.05-61-2 50 Abundance Scan 687 (11.354 mln): 30313.D (-) m/z 59.05 100.00% 59

5000

—4L lapannig 45

73

85 103

, * I • ‘ * I N 11.00 11.20 11,40 11.60

Kx l','‘ 141444a i 141414* m/ z 45.05, 55.32% miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 TT T ’ ‘ I ‘ * * TTuua • J ‘ 45 103 11.00 11.20 11.40 11.60 73 ! 31 m/z 103.05 33.56% TTITm1 1 ■ ■ ■ ■ i 111 • | ‘ i > • | । PPr 130 miz-> 30 40 50 160 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 9n8n“ t t 11** । j । i । । I 11.00 11.20 11.40 11.60

N) 5000 m/z 73.00 28.84% 31 45 103

75 80 ■ ■ । ■ ■ • ■ । ■ ■ ■ ■ । • ■ ■ ■ । ‘ । ■ ■ • ■ । ‘ । • • ■ ■ । • ■ • • । • ■ • ■ । • ■ ■ ■ । ■ miz-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087:2-Propanol, 1,1-oxybis- ■ f » ' r. । 1 । r । LTI > । । । । ■ । r

. A 59 11.00 11.20 11.40 11.60 m/z 41.00 26.92% 20.52% 31 5000 45 103 89 72 111 ■ ■ • ■ । 1 Ht pi { । i t i ■ i 1 ‘ i ■ i ■ • ■ ■ i ■ ■ ■ ■ i • I > • i • • > ■ j • . ■ • । • m/z-> 30 40 50 60 I 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

30313.D GCMS1126.M Wed Jan 02 10:17:12 2002 Page 2

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