GCMS analysis comments, sample AD29026, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC1001\29026.D Vial: 30 Acq On : 11 Dec 2001 4:58 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.92 ug/1 232431 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,3/-oxybis- 162 C8H18O3 054305-61-2 50 3 2-Propanol, 1,1 ’ -oxybis- 134 C6H14O3 000110-98-5 50 4 2 - Propanol ,/1-(2- ethoxypropoxy) - 162 C8H18O3 010143-32-5 39 Abundance Scan 695 (11.427 min): 29026.D (-) m/z 59.05 100.00% 59

5000 45 103 73 11.00 11.20 11.40 11.60 11.80 ■___________ 3911 51 . 89 , —1 1’ m/z 44.95 47*08%

£_ T-■ ■' T ■ i •1 ■ 'I • 4 • ■ TTTT . ।। । ।. miz-? 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance * ' 5#9238 2-Propanol, 1-(2-methoxy-1-methylethoxy) 59

5000 i ■ ■ ■ • i 1 ' TTTI--111111133 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.00 . 36.26% ■ i 4 ■ ■ • i * ' ■ • i1 TTTH + — ______ 130 miz-> 20 30 40 50 I60 70 80 190 100 110 120 140 Abundance * #12859: 2-Butanoi. 3,3’-oxybis- 59

11.00 11.20 11.40 11.60 11.80 5000 31 45 m/z 73.00 26.65% 103

1 134 — i i r' । । । । । । TT r । i । : TH TTTII 1 1 T 1 1 t FIIm TT 1 TIt 1 1 TT 1 1 TT TTT TT T T T T T mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1'-oxybis- 59 11.00 11.20 11.40 11.60 11.80 m/z 41.05 26.10% 5000

m/z-> ■ i ■ ■ ■ ■ 20 30 31

40 ।1 45

111 TH 50 60 72 89 103

TIIr ■ • j.» • • t ’ ■ ■ • i • * •' i • ■ • ’ i * ‘ • i • ’ • ’ i ■ 70 80 90 100 110 120 130 140 f N f * ' I' rrrr ) I I « I i 11.00 11.20 11.40 11.60 11.80

29026.D GCMS1126.M Wed Dec 12 15:46:57 2001 Page 4

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