GCMS analysis comments, sample AD28964, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0 701\28964.D Vial: 10 Acq On 7 Dec 2001 11:43 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.34 0.53 ug/1 132209 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, -(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol,/ 3,3‘ -oxybis- 162 C8H18O3 054305-61-2 50 3 2-Propa: , 1,1'-[(1-methyl-l,2-eth 192 C9H20O4 001638-16-0 40 4 2-Propa ol, 1,11-oxybis- 134 C6H14O3 000110-98-5 39 Abundance 7 Scan 686 (11.345 mln): 28964.D (-) m/z 59.05 100.. 00% 59

5000

— 51 —— 45 73

85 91 । 11 *, • । • • i • 103

' I ■■■ ■' I ■ ■ ■"' 11 • * I « • N 11.00 11.20 11.40 11.60 m/ z 45.05. 50.09% • • i •

N mlz-2 2030 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 1nt ■I ■' 1 ' ■ r' ■ ' ■ I ' ' ‘ ■ 1 1 45 103 11.00 11.20 11.40 11.60 73 31 m/z 103.05 36.06% - --- — 111 ........ - m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3’-oxybis- 59 -------- ei 11.00 11.20 11.40 11.60 5000 31 m/z 73.00 L___ - 29.02%

M 45 103

I 'i'■‘'i‘‘i■‘‘i■■ ‘ '!■‘' i ‘ !,____________ 134 ‘'i•' ■ ‘I ' • ■ ■ i ■ 1 ■ ■ i ■ ■ • ■ i ■ ■ ■ ■ i ■ • ' ■ i ■ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 #20630: 2-Propanol, 1,1‘-[(1-methyl-1,2-ethanediyi)bis(oxy)

N Abundance T I II—f • ’ 1 • I ■ ' ■ ■ J ■ ‘1' • I • 59 11.00 11.20 11.40 11.60 m/z 41.00. 25.95% 5000 31 45 103 39 | I 73........ ..... 1....... 117 । • i ■ ■ ' • i ■ ■■'ill1. —H 144MAARP miz—> 20 30 40 50 60 70 80 9Q 100 110 120 130 140 11.00 11.20 11.40 11.60

28964.D GCMS1126.M Thu Dec 13 10:20:01 2001 Page 2

NYC-WTC_000035648