GCMS analysis comments, sample AD28964, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC07 01\2 8 964.D vial: 10 Acq On 7 Dec 2001 11:43 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

11.43 0.75 ug/1 185233 1;4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-2-methoxy- 1-methylet 148 C7H16O3 020324-32-7 83 2 2-Propanol, 1,11 -oxybis- 134 C6H14O3 000110-98-5 50 3 2-Butanol, , 3 ’ -oxybis- 162 C8H18O3 054305-61-2 45 4 1-Propan , 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance 7 Scan 695 (11.427 mln): 28964.D (-) m/z 59.05 100.00% i 59

5000

• J > » * ‘ f • 39 1+t 45

1451 73

81 103

. i. • i • 1 ■ ■ i ■ 1 ■ ■ i ‘ 1 ' ■ i ■ • • ■ i ■ ■ • • i • • • • i • _N 11.00 11.20 11.40 1160 11.80 m/z 44.95 ’ 'I 11

47.48%

NX miz-? 20 30 40 50 60 7080 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy) 59

5000 TLI—TETTETT a 45 73 103 11.00 11.20 11.40 11.60 11.80 31 m/z 103.05 34.85%

miz- 20 —mm 30 40 50 60 70 80 ‘ "90“ ‘ 100 110 120130′ 140 ........................... !........................ 130...........

Abundance #6087: 2-Propanol, 1,1-oxybis- 59 —PIITTT_1_1_1_r Ir • J TM 11.00 11.20 11.40 11.60 11.80 31 45 m/z 73.00 28.07%

M- 5000 103 89 72 — • i ■ • • • i • ■ ■ ■ i ■ ■ ■ ■ i ■ • • ■ ik ‘ ■ i • •' • i • ■ ■1 i1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- I TITTur 1 1 1 1 ' 1 * t ‘ ' 1 ' 1 ’ 1 ‘ 59 11.00 11.20 11.40 11.60 11.80

.J m/z 41.05 24.65% 5000 31 45 103

- # T-r-j-r — 1‘ ‘ ।•■1■।■'> •। ■ ■ ■ • । • 1 • • i ■ ■ ■ • i * ■ • ■ i 134 • • 1 ■ i • -AA-PP95495 - m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

28964.D GCMS1126.M Thu Dec 13 10:20:06 2001 Page 3

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