GCMS analysis comments, sample AD28964, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\28964.D Vial: 10 Acq On 7 Dec 2001 11:43 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.37 ug/1 834933 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silane, tet amethyl - 88 C4H12Si 000075-76-3 47 2 N-Ethylfo: mi de 73 C3H7NO 000627-45-2 9 3 Pentane, . -methoxy- 102 C6H140 036839-67-5 9 4 1,3-Dioxplane, 2-pentadecyl- 284 C18H36O2:__ 004360-57-0 9 Abundance Scan 279 (7.608 min): 28964.D (-) m/z 73.00 100.00% I 73 5000 43 i ■ ‘ • i ' ■ ' ■ i 1 ‘ ' i

87 103 7.20 7.40 7.60 7.80 8.00 38 I, I 50 55, 60 67, , • • । ■ ■ i ■ • • • I 1 FTTTTTtr I'1 1 1 1 T’t j । • m/z 43.05 26.62% miz-? 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 T TT 7.20 7.40 7.80 7.80 8.00 45 m/z 41.00 9.92% ’ • I ‘ 15 ' I , .1 53 59 । 88 FTmTTTEHTTugtt • • i • ■ ‘ ■ i ' ■ ‘ 1 i 1 ' ' ' i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292; N-Ethylformamide 30 73 TTTTTTTTrrr । 7.20 7.40 7.60 7.80 8.00 5000 m/z 44.95 9.42% 44 58 ! 1 15 miz—> ■ ' i ■ • ■ ■ i 1 10 20 L 30 40 l— 50 60 70 • • i ■ 1 • ' i ■ ■ ' • i 1 ■ • 1 i ■ ■ ■ b i 1 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 1 hi । । it । 1TTT > . -j i . 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0.0 6.44%

5000 45

27 33 3,9, — — — ■ ■ i ■ ■ ■ • i ■ ' ' • i 1 • ■ ‘i 1 ‘ ‘ ■ । 55 ■ i ■ •11 r* । ■ i • • ■ • i • ■ ■ ■ i ' ' ' ■ i •

m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

28964.D GCMS1126.M Thu Dec 13 10:19:57 2001 Page 1

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