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GCMS analysis results for sample AE02966, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02966 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005627–000005641

Folder label: “GCMS X 2/7/02 A 2/9/02”

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Scanned page image, NYC-WTC_000005634
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\FEB0802\2966.D Vial: 30 Acq On 9 Feb 2002 1:30 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

8.22 2.34 ug/1 254656 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 38 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 3 Pentane,/3-methoxy - 102 C6H140 036839-67-5 9 4 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 Abundance ' Scan 346 (8.218 min): 2966.D (-) i m/z 72.9,5 100.00% 73

5000 43

7.80 8.00 8.20 8.40__ 8.60 1 1 11I1 1 50 ,1 138.1) 1 , 1 1 1 1.. * 1 1 1.1 1 , 87 103 '■ I 1 1 1 1 I 1 1 1 1 I 1 1 av m/z 43.05 38.89% m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 7.80 8.00 8.20 8.40 8.60__ 45 m/z 45.05 13.19% 15 I 53 1'59 -- ■ ' i ■ ■ 1 ■ i 1 ■ ■ ■ i ' ■ ■ ■ i 1 ■ ' ■ i ■' ■ 1' I 1 1 1 1 I 1 m/z->10 20 30____ 40 50 60 70 80 90 100 110 Abundance 73 .................. .

5000

45 55 m/z 77QTT 7.80 8.00 8.20 8.40 8.60

27 87 39 ■ ■ i ■ ■ ‘ ■ i ' 1 ■ ■ i TI m/z-> 10 20 30 40l 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73 7.80 8.00 8.20 8.40 8.60 ■ m/z 39.05 6.87% 5000 45

m/z-> 10 .. 27,23.38.. 20 30 40 ' i ■ 50 55 ‘ i 1 ' ' ' I1 ' 1 ' i ' ' 1 1 1 1 ' 1 ' 1 1 1 1 1 1 1 60 70 80 90 100 110 7.80 ................ I 8.00 8.20 X............... 8.40 8.60

2966.D GCMS0208.M Wed Feb 13 11:07:22 2002 Page 1

NYC-WTC_000005634

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NYC-WTC_000005634Source: NYC Law Department, mirrored locally

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