GCMS analysis results for sample AE02969, February 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\ FEBO 8 02\2969.D Vial: 33 Acq On 9 Feb 2002 4:25 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.22 2.40 ug/1 295924 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 38 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Pentane, 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance Scan 346 (8.219 min): 2969.D (-) m/ z 73.00 100.00% 73

5000 43

................ 38 I |50 55 , , , 67 I 1........ 87...........103 7.80 8.00 8.20__ 8.40 8.60 11i111 > i■111i■1 r'n11■।111 ‘I 1 1 1 1 1 । m/z 43.05 39.46% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Siiane. tetramethyl- 73

5000 7.80 8.00 8.20 8.40 8.60 45 m/ Z 45.05 13.77% 15 ! 53 59 I 88 ■ ■ i ■ ■ • ■ i • > ■ ■ i • > < ■ i ■ • • । l 1 ■ ■ i‘। i 1 > > I i 1 ■ ■ i ■ ■ ' 1 i ■ ■ ' 1 1 1 1 1 1 1 1 m/Z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 73 i ■ • ■ ■ i ■ ■ 7.80 8.00 8.20 8.40 8.60 5000 m/ z 41.05 12.49% 55 45 87 27 ' 1 i 1 ' ' 1 1 1 1 1 1 1 1 ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 00 m ।n । । । । 30 7.80 8.00 8.20 8.40 8.60 m/Z 71.00 7.36% 5000

41 1* 15 I30'' ' 140’* 1 50 55 60 ■ j ■ ■■■ • I ‘ ‘ । 70 | ■ 1 87 i ■ ' ' ' i ' ' m/z-> 10 20 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

2969.D GCMS0208.M Wed Feb 13 11:09:52 2002 Page 1

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