GCMS analysis results for sample AE03014, February 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\FEB 0802\3014.D Vial: 38 Acq On 9 Feb 2002 9:15 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.22 2.15 ug/1 332132 1,4-Dichlorobenzene-d4 12.35

Hit# Of 5 ntative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 47 2 1,3-Dioxolane, 2- (3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 40 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 Abundance Scan 346 (8.217 min): 3014.D (-) m/z 73.00100.00% 73

5000 43

m/z-> ■ ■ i ■ ■ > > i ■ ■ ■ ■ । ■ 10 20 30 40 50 60 70 80 , 87 uuiv di’ IIIII11II* 90 100 103 110 120 m/z 117 7.80 _ 8.00 8.20 8.40 8.60

Abundance #62932: Silane, tetramethyl- 73

5000 7.80 a nnmn .-I . I . , 8.00__ 8.20 8.40 8.60 45 m/z 45.05 14.84% 15 53 59 88 • ■ । l l i > । ■1 ■ ■ < • i' i • • • ■ i ■ 1 ■ ' i ' ' ' ' i ' ■ ' ■ i ■ ' ■ ■ i ■ ■ ■ ■ i ‘ ‘ m/z->10 20___ 30 40 50 60 70 80 90 100 110 120 Abundance 73

7.80 8.00 8.20 8.40 8.60 5000 m/z 41.05 12.93% 45 36 55 67 ................ 109115 ' i ' ■ ■ ' i ‘ 1 ■ ■ i ■ ' ' ' i ' ■ ‘ ' i ' m/z->.. ........ 10 20 30 40 50 60 70 80 90 100 110 120 1, Abundance #763: 1-Butanamine, 3-methyl- 1 ' i ' ' ■ ‘T7 30 7.80 8.00 8.20 8.40 8.60 m/z 7.31% 39.05 5000

41 m/z-> ■ ■ । 10 15 ■ i ' ' ' h " 1 ’ 20 30 55 70 ।''i'''■i'''■I'''■i'' 40 50 87 60 70 80 90 100 110 120 7.80 PIPi 8.00 48.40—fr 8.20 8.60 '

3014.D GCMS0208.M Wed Feb 13 11:13:33 2002 Page 1

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