GCMS analysis summary, sample AD31365, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31365.D Vial: 22 Acq On : 16 Jan 2002 7:30 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.45 ug/1 1050060 1,4-Dichlorobenzene-d4 11.50

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 1,3-Dioxolane, 2-pentadecyl- 284 C18H3602: 004360-57-0 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 1-Butanamine, 3-methyl- 87 C5H13N _ 000107-85-7 7 Abundance Scan 262 (7,450 min): 31365.D (-) m/z 73.00 100.00% 73

5000 43 — 7.201 7.40 7.60 7.80 0- si.57.1 tTIT* 87 103—gnmTD*)DLUTTET rn/z 43.0,0 33.12% miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #62932: Silane, tetramethyi- 73

5000 1 1 ■ • i 1 ■ 1 ’II4I4I3 |-i । । 7.20 7.40 7.60 7.80 45 m/z 45.0,5 12.00% । 15_____ J 59 88 m/z->_ ■ i ■ ■ ■ • i 20__40 60_ 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191 1 3-D-oxclere. 2-pontadecy]. 73 r..r , c 1 ■ i ."i 1- । 7.20 7.40 7.60 7.80 5000 m/z 41.00 11.82%

43 57 86 99 256 283 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #1793: Pentane, 3-methoxy- —PrTm—TT 73 7.20 7.40 7.60 7.80 m/ z 71.00 7.18% 5000 45

27 . . । 1 . । . . , 59 ’I , BI4TFI/IIII141 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.20 7.40 7.60 7.80

31365.D GCMS1126.M Mon Feb 04 15:04:18 2002 Page 1

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