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GCMS analysis results for sample AD31457, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31457 conducted on February 13, 2002.

NYC-WTC_000018353–000018361

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018360
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JANI602\31457.D Vial: 14 Acq On : 17 Jan 2002 12:20 am Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.67 ug/1 1243170 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 3 Butane ,/2-methoxy-2 -methyl - 102 C6H140 000994-05-8 9 4 Pentane, 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance Scan 262 (7.447 mln): 31457.D (-) m/z 73.0,0 100.00% 73

5000 43 I’II’I’II |TTt 7.20 7.40 7.60 7.80 mlz-> +74 >'11 “ 87 103 11a‘sa‘6tajsaastdasss*1*A1*1******(*1** 20 40 60 80 100 120 140 160 180 200 220 240 260 280 m/z 43.00 32.51% Abundance #62932: Silane, tetramethyl- 73

5000 .... —11), rrr 7.20 7.40 7.60 7.80 45 m/z 45.00 12.06% 15 59 1 TPTri J"• l" 88 . ...... m/z-> 20 40 60 ' 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191 1.3-Dioxolane. 2-pentadecyl 73 ----- 7.20 7.40 7.60 7.80 5000 m/z 41.00 11.56%

i 43 57 ; 86 99 256 283 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #1761: Butane, 2-methoxy-2-methyl- ———— 73 7.20 7.40 7.60 7.80 m/z 71.00 6.61% 5000 55 87 27 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.20 7.40 7.60 7.80

31457.D GCMS0103.M Thu Feb 07 09:18:05 2002 Page 1 NYC-WTC_000018360

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NYC-WTC_000018360Source: NYC Law Department, mirrored locally

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