GCMS analysis results sample AD29459, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\29459.D Vial: 26 Acq On : 13 Dec 2001 3:21 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 3.64 ug/1 953278 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetr methyl- 88 C4H12Si 000075-76-3 25 2 N-Ethyl form. ide 73 C3H7NO 000627-45-2 9 3 1,3-DioxolaTie, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 'Abundance Scan 278 (7.593 min): 29459.D (-) m/ z 73.00 100.00% 73

5000 43 7.20 7.40 7.60 7.80 8.00

miz-> i • ■ ■ ■ । > 10 20 — 30 34 40 1 55 61 67, । । • +— 87 11 ' I TIrTT . 50 60 70 80 90 103 100 110 120 m/z 43.0.0 27.74% Abundance #62932: Silane, tetramethyl- 73

.......... ............. 5000 7.20 7.40 7.60 7.80 8.00 45 m/ z 44.9, 10.14% 15 | 53 59 88 ...... 1 m/z->10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73 ■ 'i ■ ■ ■ 1 i ■ 1 1 TTTT । । h . । 7.20 7.40 7.60 7.80 8.00 | 5000- m/z 41.0.0 9.34% 44 58

15 I ,1 ' i ■ < ■ i ■ • ■ ■ i ■ ' i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet TTmu/r TT 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.89% 5000- 45

................. 36 11 ■ ■ i ■ ' ■ • i ■ 1 ■ ■ i ' ■ 1 ■ i ■ 1 55 67. - ' ■ i ' '' ' i 1 ' ' ''i • 109 115 m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 3.00

29459.D GCMS1126.M Fri Dec 21 12:26:23 2001 Page 1

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