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GCMS analysis results sample AD29457, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD29457 conducted on January 4, 2002, showing unknown compounds and surrogates.

NYC-WTC_000036425–000036435

Folder label: “GCMS X 12/5/01 A 12/12/01

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Scanned page image, NYC-WTC_000036432
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\29457.D Vial: 17 Acq On : 12 Dec 2001 6:36 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr': 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 2.95 ug/1 896611 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, te ramethyl - 88 C4H12Si 000075-76-3 9 2 N-Ethylfo lamide 73 C3H7NO 000627-45-2 9 3 1,3 -Dioxo ane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Butane, /2 -methoxy-2-methyl- 102 C6H140 000994-05.-8 9 'Abundance Scan 278 (7.594 min): 29457.D (-) m/z 73.0,0 100.00% 73

5000 43 87 103 7.20 7.40 7.60 7.80 8.00 37, | | 49 55 50 67, , ■ ' i ■ ' ' ' i 1 > । • ■ । । । । । > . । .... । . . . > । . l ■ ■ i ■ 1 I 1 m/ z 43.00 27.33% m/z-> 10 20 30 40 50 60 70 80 90 100 110 • 120 Abundance #62932: Silane, tetramethyl- 73

5000- 1 i ■ • ' ■ i ' P 7.20 7.40 7.60 7.80 8.00 45 m/ z 44.95 10.48% 1.5 I 53 59 I............88 — t PH । .... । . m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73 ' I ' ' ' 1 'I Ir . r । . . 7.20 7.40 7.60 7.80 8.00 5000 m/ Z 41.00 9.32% 44 58

15 1 . ! miz-> 10 20 30_40 50 60 70 80 90 100 110 120 'Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 l • ' 1 1 1 1 7.20 7.40 11 — TOInur T TT 7.60 7.80 3.00 m/ z 71.00 6.25% 5000- 45

......................... 36 il i ' ' ' ■ i ■ ' ' ' i ' ' 1 ' i ■ 55 67. ■ I < •'< - I ■ ‘ • 'I ’ ................................. 109 115 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29457.D GCMS1126.M Fri Dec 21 12:24:11 2001 Page 1

NYC-WTC_000036432

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NYC-WTC_000036432Source: NYC Law Department, mirrored locally

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