GCMS analysis results sample AD29289, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\29289.D Vial: 24 Acq On 13 Dec 2001 1:25 am Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 3.73 ug/1 1099440 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane/ 2 - (3-bromo-5,5,5-tri 352 C10H16BrC1302 000000-00-0 9 4 Pentane, 3-m/thoxy-__________________ 102 C6H140 036839-67-5 9 Abundance Scan 278 (7.594 min): 29289.D (-) m/ z 73.00 100.00%

A 73

5000- 43

|.......... 87 ............. 103...................... 7.20 7.40 7.60 7.80 8.00

m/z-> 10 20 30 37, |, | 50 55 60 • ■ l' 1 1 •i ' ■ ■ ■ i • 40 50 60 6770— 80 90 100 110 120 m/ z 42.95 27.33% Abundance #62932: Silane, tetramethyl- 73

5000 7.20 7.40 7.60 7.80 8.00 45 m/ z 4 5.0.5 10.79% 15 • । ■ • • • । • I 53 59 I 88 ■ ■ i ■ ''' ----- ' i 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292; N-Ethylformamide 30 73 --- 7.20 7.40 7.60 7.80 8.00 5000 m/ z 41.00 9.81% 44 58 i 15 | | I , r-j-n-i-r-|-r-r-r . । . . . > । . > nn m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.27% 5000- 45

................. 36 11 1'। ■ 55 67. ■ । ■ ■ ■11 ■ +r 109 115 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29289.D GCMS1126.M Fri Dec 21 12:17:57 2001 Page 1

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