GCMS analysis results for sample AD30113, Jan 2002

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Data File : C:\HPCHEM\l\DATA\DEC1901\30113 .D Vial: 13 Acq On : 20 Dec 2001 1:10 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.78 ug/1 1028390 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 entative ID MW MolForm CAS# Qual 1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 4 1,3- ioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 279 (7.604 mln): 30113.D (-) m/z 73.0,0 100.00% 73

5000 43 i ‘ ' ‘ 1 I • • ■ ■ i • • • • i 7.20 7.40 7.60 7.80 8.00 ...................................... iU, 5055..61. 67,1, i, ■ ■ i ■ ‘ 87* j - ■ ■ ‘ i 103 •’* * ■ i * m/z 43.00 29.09% m/z-> 10 20 30 40 50 ’ 60 ' 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 1*118*** 1 • i । * 7.20 7.40 7.60 7.80 8.00 45 m/z 45.05 10.77% 1 15 53 59 , 88 ■ ■ • i ■ ''' 1 i 1 1 1 ' i 1 PTT i * 1 • i i । ■ ■ ■ ■ । 1 ■ **14**I**I1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 y-.-i-.-rr-. T144I4I 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.0,5 10.09% 44 58 15 J : I1III**000*1* miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- inop* . . . 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0,0 6.58% 5000 55 87 45 27 33 JL - ■ ' i ■ 1 ' ■ i ■ ■ ■ • i ■ ■ ■ ■ i ' ■ ■ ■ i ■ • 1 ■ i 1 1 11411 a ‘ •p"1 1 < l l • m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30113.D GCMS1126.M Wed Jan 02 16:06:54 2002 Page 1

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