GCMS analysis comments, sample AD29287, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29287.D Vial: 17 Acq On : 11 Dec 2001 2:20 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.35 0.97 ug/1 255982 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3’-oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1,1 ’ - [ (1-methyl-l, 2-eth 192 C9H20O4 001638-16-0 42 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 42 Abundance Scan 686 (11.345 mln): 29287.D (-) m/z 59.00 10 .00% 59

5000

•। • — 45

tpngT 85 73 103

,1...... 130............ ■ • • i ■ ■ ■ i • ■ ■ ■ i ■ ‘ ■ • I ■ •1' i1 • •1111 ■ “ i111 ‘ i ■ ■ t ■ • _ML 11.00 11.20 11.40 11.60 m/z 45.05, 48.19% miz-? 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 1 1 TTT ■ । । < ' 1 r1 1 1 1 i 1 ■ 11 i 1 45 11.00 11.20 11.40 11.60 73 31 m/z 103.00 34.90% ; • | ‘ ■ > । T TI II TI - — 130 i'1 ‘11'' I ‘ ‘ t T T miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance .... #12859: 2-Butanol. 3,3°-oxybis- 59 ■ ■ i ' ' ■ T T T 11.00 11.20 11.40 11.60 5000 31 m/z 73.0.0 0 30.09%

A 45 103

. ।; TTT. > T]।।. 134 T i■•••i ■ I"1 ’I TT 1 ''611'111 miz-? 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #69286:2-Propanol, 1,1‘-[(1-methyl-1,2-ethanediyi)bis(oxy) ‘ • J ' • • • 1 » T T pi i 59 11.00 11.20 11.40 11.60 m/z 41.05 __ ____ 24.29% 5000

31 103 45 117 — . 73 | 133 ' i11 ■ • i ■ “ 1161 ■।11 ।■ Tpumpku ■ ’ i “ “ i ‘ 1-' ■ • • i Tf1 T — Ts I C 8 I : I I I m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.00 11.20 11.40 11.60

29287.D GCMS1126.M Fri Dec 14 16:14:19 2001 Page 2

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