Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
NYC-WTC_000036126–000036136Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29287.D Vial: 17 Acq On : 11 Dec 2001 2:20 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
7.60 3.44 ug/1 909961 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 Abundance Scan 278 (7.600 min): 29287.D (-) m/z 73.00 100.00% 73
5000 43 • I ‘ 1 ' ' I • 1 1 1 i ' 1 1 1 i 37, I, | 50 55 . 67, । 87 I I 1 103 7.20 7.40 7.60 7.80 8.00 0 1 ■ i 11 11 I '' 1 1 1 1 TITT r> t I I 1’’ ■ • i ■ i ■ ■ ‘ • i • • m/z 43.05 27.12% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73 TI—TTTTT 5000 7.20 7.40 7.60 7.80 8.00 44 58 m/z 41.00 10.50% 15 miz-> — 1020 30 '40T50 — 60I1'1 1 '1701 TTT[T t TTI T 1 1 1111181 80 90 100 110 120 Abundance #62932; Silane, tetramethyl- 713 — — ■ I' r r l' — -------
7.20 7.40 7.60 7.80 8.00 5000 m/z 44.95 10.05% 45 15 53 59 .............88.................................. —ma T———BmmTTi miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet ITaunpnnmmDDTmgun 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.20%
5000 45 36 1 । 55 gr TTTTTPpnT ' i 1 ' ■ • i ■ ■ 67. 1 ■ i ■ _______________ 109115 T LIT TI I J I I T1TT I I I I I ! T168 11’1111TrrTXTIIrr miz—> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00
29287.D GCMS1126.M Fri Dec 14 16:14:15 2001 Page 1
NYC-WTC_000036133
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NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036447
Laboratory report documenting GCMS analysis of sample AD29459 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036029
Laboratory report noting GCMS scan results for sample AD29140 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036480
Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035820
Lab notes for sample AD29022 indicate no unusual compounds detected but one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
Filed in the same folder
NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
Filed in the same folder
NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder