Laboratory report noting GCMS scan results for sample AD29233 with phthalates and nonadecanol detected.
NYC-WTC_000036137–000036150Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC1001\29233.D Vial: 15 Acq On : 11 Dec 2001 12:23 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
7.59 3.71 ug/1 1134650 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 278 (7.594 mln): 29233.D (-) m/ z 73.00 100.00% 73
5000 43 • i ' ' • ' i ■ 1 ■ 1 i ■ ‘ ‘ i T 1 i 1 7.20 7.40 7.60 7.80 8.00 ____________ 36, |,... ......... . , 87 103 TT-J- >>■•!>■ TTT8 VI ft > • * i • • ‘ • । • ‘ • ■ । ■ । • • ■ ■ । b ■ m/z miz-> 10 20 30 40I 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73 - 5000 -1110/218 58 7.20 7.40 7.60 7.80 8.00 44 m/z 44.9.5 9.56% ■ • i ■ 15 ■ • ■ i ■ ■ ■ ■ ■ ■ i'I'I'I ■ i ■ I • • 1 ‘ I ‘ 1 ‘ ‘ I ■ ‘ 1 ‘ I ‘ ' 1 ' ■ ‘ ' I ‘ ‘ 1 ' I ' ‘ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423:1.3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 r 11 7.60 — * r 7.40 7.20 — —rr 11 ( — 7.80 8.00 5000 m/z 41.00 9.39% 45 36 55 67 109115 IIBTTrr • • i ■ 1 ■ • i • ' • ■ i ■ ■ 1 • i ‘ 13) T-rT-rv-T-r-t-r'-f-rh-. m/z- 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63573: 3-Pentanol, 3-methyl- "TTTTT 73 7.20 7.40 7.60 7.80i 8.00 m/z 71.0.0 6.11% 5000 55 45 87 27 ■ • i • ' ' ' i ' ' ■ ■ i ‘ 39.1.. , ..... .... ....... ...... > • * । • । . । i . । . . . • । i i b > t . . m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00
29233.D GCMS1126.M Fri Dec 14 16:12:48 2001 Page 1
NYC-WTC_000036144
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NYC-WTC_000036079
Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036311
Laboratory analysis report for sample AD29285 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017796
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30354 conducted on January 10, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
Filed in the same folder
NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
Filed in the same folder
NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder