GCMS analysis comments, sample AD29233, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29233.D Vial: 15 Acq On : 11 Dec 2001 12:23 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

7.74 0.77 ug/1 235995 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 40 2 Nonadecanol 284 C19H40O 052783-43-4 9 3 1-Hexadecanol 242 C16H340 036653-82-4 9 4 Nonane, 4,5 -dimet hyl- ___ 156 C11H24 017302-23-7 7 Abundance Scan 294 (7.741 mln): 29233.D (-) m/z 43

5000 112B T-T-f

83 97 7.40 7.60 7.80 8.00

miz-> — , 1 63 20 40 60 1 ’Itt 80 100 110.117—— 120 140 160 180 2' ( 22o' 240 260 m/z 124.85 7.39% Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 —...A 7.40 7.60 7.80 T 8.00 T

15 m/z 126.9.0 6.53% 85 97 125_______________ ____ —TIT miz-> 20 40 60 ' ' 80 100 120 140 160 180 200 ‘226' 240 260 Abundance #40237 Nonadecanol 43 57 ' I ■ - । । ■ । . T 7.40 7.60 7.80 8.00 5000 m/ z 96.95 6.16% 31 71 2397 I- • 111 1 125 252 266 ■ ■ • । ■ • • • । • "I" ' • i 1 ‘ ' 1 1 ' ‘‘ 1 ■ • ■ ■ i • • ' ■ i • ■ • ■ i ■ ■ ■ ■ i ■ ■ • • i ■ • ■ ■ i'1 • ■ i ‘ ‘ miz-? 20 40 60 80 100 120 .140 160 180 200 220 240 260 — Abundance #71247:1-Hexadecano! ■ ' i • ■ ■ ' i ‘ • I • ‘ ‘ ‘ I 43 55 T 7.40 7.60 7.80 8.00 m/z 82.8,5 5.94% 5000 83 27 70 97

miz-s 111 • ■ •11 • ■ 118 60 । 125 . । 111■ 1 196 224 ■ i ■ ■ • • । ■1111 ■1 ■111 ■ • ■ । ■1 * ■ 1 *1 AAAALWAA 20 40 80 100 120 140 160 180 200 220 240 260 7.40 7.60 7.80 8.00

29233.D GCMS1126.M Fri Dec 14 16:12:53 2001 Page 2

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