GCMS analysis results for sample AD30352, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.

NYC-WTC_000017808–000017832

Folder label: “GCMS X 12/13/01 A 12/27/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\DEC2701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

7.76 0.54 ug/1 173270 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 25 2 1-Fluorononane 146 C9H19F 000463-18-3 9 3 Hexyl octyl ether 214 C14H30O 000000-00-0 9 4 4-Penten-2-one 84 C5H80 013891-87-7 4 Abundance Scan 296 (7.759 min): 30352.D (-) m/z 42.95100.00% 43

5000 1141 » I I I » I I I » I I I I I J [4

■ ■ I ' 1 ■ ' l oer 37 1 151 11. 63. 69 $4 . ।.... । ili. (.. 97 । । 119125 7.40 m/z 124.85 7.60 7.80 8.00 10.04% 8.20 i , m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 7.40 7.60 7.80 8.00 8.20 15 m/z 42.05 7.28% | 35 i .49 85 97 117 125 ■ ■ i • ■ ■ ■ i • ■ 1 ' i ■ ■ • ■ i ■ 1 1 1 i ■ ' ■ ‘ i ■ ■ ' ' i ■ ■ 1 ■ i Tt ' i • ' ■ • i ' ■ 1 ■ i ■ ■ ■ ■ i ■ ■ ■ • i 1 ‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8922: 1-Fluoroponane 43 *TRPPaTerrrTr 7.40 7.60 7.80 8.00 8.20 5000 m/z 83.85 7.10% 56 27 33 . .।।।।1111 70 84 97 MVVAmPWiniondya *. i*...i..‘*i*...i*...।...»i .. .. i.... i * m/z-> 10 20 30 40 50 60 70 80> 90 100 110 120 130 Abundance #26415: Hexyl octyl ether 43 57 85 7.40 7.60 7.80 8.00 8.20

,J . 71 m/z 84.95 6.70% 5000

■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ ' ■ i •' i11 11 ■ ■ 111 ■ ■' ।1 ... 103. . 112 . M—A-AYAAAA--A miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.80 7.80 8.00 8.20

30352.D GCMS1126.M Wed Jan 02 10:50:19 2002 Page 2

NYC-WTC_000017817

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NYC-WTC_000017817Source: NYC Law Department, mirrored locally

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