Laboratory report noting GCMS scan results for sample AD29233 with phthalates and nonadecanol detected.
NYC-WTC_000036137–000036150Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC1001\29233.D Vial: 15 Acq On : 11 Dec 2001 12:23 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Ethanol, 2-butoxy- Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
9.22 0.71 ug/1 216970 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Ethanol, 2-butoxy- 118 C6H1402 000111-76-2 83 2 2-Butanol, 3,3-dimethyl- 102 C6H140 000464-07-3 17 3 Isobutyl ether 130 C8H180 000628-55-7 17 4 Propanoic acid, 2-methylpropyl este 130 C7H14O2 000540-42-1 12 Abundance Scan 455 (9.219 min): 29233.D (-) m/z 57.0,0 100.00% 57
5000 45 87 11232m T7 ’ TT i : 1 ; DIrT 39 1 100 8.80 9.00 9.20 9.40 9.60 .. 114451 14 6363.69.78 1PTT • i • • • • i m/z 45.05 40.71% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64441: Ethanol, 2-butoxy- 57
5000 0 1 —2 1 l —Yr ? - = 45 8.80 9.00 1 9.20 ' 9.40 ' 9.60 27 87 m/z 41.05 33.02% , 75 118 Tr-p-m-j l I l . 1 . . .jrr - ■ i' ■ ■ ■ i ■' ■ 100 ■ I ■ • • • i ■ • ■ ■ i ■ ■ • ■ i ■ • •11 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #63574; 2-Butanol, 3,3-dimethyl- 45 57 |i rii jilt i j i » »' » । i i i i | TT 8.80 9.00 9.20 9.40 9.60 5000 m/z 87.00 19.64% . 15 27 69 87 102 ■ T1900t—u——TT-TTTTETT-ITTIIISIs I TT ‘ ‘ । m/z->__ 10__ 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5524: Isobutyl ether ■ ■ i ■ ■ • ■ i • ■ ■ ■ i ‘ ’ TIT 57 8.80 9.00 9.20 9.40 9.60 m/z 56.00 9.45% 5000 . /...............
87 27 43 73 | 130 TII । । < -i i i'i 11 । TTITIr TO—’-1—3’ITr TTPTITUTNT mlz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 8.80 9.00 9.20 9.40 9.60
29233.D GCMS1126.M Fri Dec 14 16:12:57 2001 Page 3
NYC-WTC_000036146
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NYC-WTC_000036079
Laboratory report showing GCMS scan results for sample AD29135 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036311
Laboratory analysis report for sample AD29285 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035919
Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035978
Laboratory report noting detection of di-n-butylphthalate in sample AD29026 analyzed on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035955
Laboratory report documenting GCMS scan results for sample AD29137 with no unusual compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017796
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30354 conducted on January 10, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
Filed in the same folder
NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
Filed in the same folder
NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder