GCMS analysis results, sample AD29135, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC1001\29234.D Vial: 23 Acq On : 11 Dec 2001 8:10 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Ethanol, 2-butoxy- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

9.22 1.01 ug/1 254003 1,4-Dichlorobenzene-d4 11.68

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2 -butoxy- 118 C6H14O2 000111-76-2 83 2 1-Butene, 4-butoxy- 128 C8H160 034061-76-2 23 3 Isobutyl ether 130 C8H180 000628-55-7 17 4 n-Butyl ether 130 C8H180 ________ 000142-96-1 17 Abundance Scan 454 (9.215 min): 29234.D (-) m/z 57.00 100.00% 57

5000 45 87 39 1451 163 75 100 8.80 9.00' 9.20 9.40 9.60 ‘ I 1 ‘ 1 ‘ P 1 ‘ 1 -' Tgr I I I I I I I ] I ...... H 1 I m/z 44.95 38.70% miz-? 20 30 40 50 60 70 80I 90 100 110 120 130 Abundance #64439: Ethanol, 2-butoxy- 57

5000 TTif 45 8.80 9.00 9.20 9.40 9.60 87 m/z 41.0,5 36.37% 27 75 1 100______ 118 ______ I i_______ — — • 1i■• • ■I • • ■ • i■■ 1• i• 4 ■■ i• • • ■ i TTTurr i. . . . । . miz- 20 3040 50 60 70 80 90 100 110 120 130 Abundance............ #5107: 1-Butene, 4-butoxy- 57 TTPTTTTTT 8.80 9.00 9.20 9.40 9.60 5000 m/z 87.10 19.20% 41 87 ----- r-[ 1111’2’311 T miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5524: Isobutyl ether T -1 1? I । > ■ 57 8.80 9.00 9.20 9.40 9.60 m/z 56.00 10.36% 5000

27 43 , „...... 73 87 TTT T T I IT I v I l' 1189 J I I I L p>■।p■>■p■ ■ ■ p■ ■ 130 ■ I* ■ ■ ■ । 8.80 9.00 9.20 9.40 9.60 miz—> 20 30 40 50 60 70 80 90 100 110 120 130

29234.D GCMS1126.M Fri Dec 14 16:48:38 2001 Page 3

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