GCMS analysis results, sample AD29135, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC1001\29234.D Vial: 23 Acq On : 11 Dec 2001 8:10 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 7.74 0.47 ug/1 117625 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 25 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 3 Cyclobutanol, 3-ethyl-, acetate 142 C8H14O2 056335-72-9 4 4 2-Butyne-1,4-diol, diacetate 170 C8H10O4 001573-17-7 4 Abundance Scan 293 (7.737 min): 29234.D (-) m/z 4 .95 100.00% 43

5000 TI । > । l t I 18B.T I IT I 1 ( 125 7.40 7.60 7.80 8.00 99 miz-> 10 120— 30 —H+ 37 40 50 60 70 80 90 J I 117 || 100 110 120 130 m/z 124.95 11.79% Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 T T 7.40 7.60 7.80 8.00 15 m/z 127.00 9.05% | 35 | 49 85 97 117 125 TBImuTugTTTTT miz-> ' 10 120 30 2 40 ' 50 60 70 80 90 100 110 120 130 Abundance #4732; N-Acetylpyrrolidone 43 • » i ' * * < j » * ■ i • ‘ ■ 1 i • ‘ ■ i 7.40 7.60 7.80 8.00 5000 m/ z 81.85 7.64% 99 127 30 56 86 69 —mm ■ । ■11 ■ ■ • • । • TIt _12 ■ • i •' ■ ■ I • ■ •11 ■ ■ ■ ■ i ■ ■1TT 111 > ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance ................... . #7909: Cyclobutanol, 3-ethyl-, acetate ■ ■ I * * ‘ ■ i ‘ > ■ i * • » • i * * * * i 43 7.40 7.60 7.80 8.00 m/z 46.85 7.20% 5000 86 MWWyWwwo —mmm+ ,+ l l'!58h l , 67 99 1 TH I[IIneTc-Tu 114 —sCs8ItI[I8 TImnm—mT m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.60 7.80 8.00

29234.D GCMS1126.M Fri Dec 14 16:48:33 2001 Page 2

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