Repeat gas chromatography-mass spectrometry analysis of sample AD28596 after re-extraction, confirming bis(2-Ethylhexyl)phthalate at 0.36 ug/L with improved standard recovery of 89
NYC-WTC_000034908–000034918Folder label: “GCMS X 11/23/01 A 11/29/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC1001\28596.D Vial: 21 Acq On : 11 Dec 2001 6:14 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
11.42 1.29 ug/1 319306 1,4-Dichlorobenzene-d4 11.67
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 50 3 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 47 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance Scan 694 (11.418 min): 28596.D (-) m/z 59.05 100.00%
5000 45 73 103 AL 11.00 11.20 11.40 11.60 11.80
m&~> 20 ' i ■ ' ■ ■ i ' 30 -al51—— 89 ' TPrT I ' TIT " " T , 130 ' i■'■■i•■•■i'1■■i■ m/ z 44.9,5 41.71%
UA 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59
5000 I 1 1 1 .............. I > I I > I > I I I I 45 103 11.00 11.20 11.40 11.60 11.80 73
.s. 31 m/z 103.00 32.96% —— ।............. 130 mfz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- 59 11.00 11.20 11.40 11.60 11.80 5000 31 m/ z 73.00 28.43% 45 103
miz-2 Abundance 20 ' । ■1111 ■'11 ■ • • 30 40 I iI 134 TT" ' 1 1 i 1 ■ ' ' I 1 1 1 1 I r' 1 TIT । । । । । ir 1 1 1 ' ■ ■ i 1 1 ■ 1 i ■ r ' ■ i 1 50 60 70 80 90 #9233:2-Propanol, 1-(2-methoxypropoxy)- 59 100 110 120 130 140
m/z 41.05 VN TTr I 1 1 I' ' I ' ‘ 1 1 I ' 1 1 1 I ' 1 11.00 11.20 11.40 11.60 11.80 23.30%
UN 5000
31 45 73 104 ...... 1..... 41...... 4— — j____________ Ir_________ 130 1 1’’’’ TT I I I | I I I r | l ■ | ! > < > | I I I > | 1 ■ I I | | TTTTTTT ■ l • • ■ ■ l ■ • • ■ I ■ > m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80
28596.D GCMS1126.M Fri Dec 14 16:47:13 2001 Page 3
NYC-WTC_000034917
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035651
Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036480
Laboratory report documenting GCMS analysis of sample AD29462 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000034718
Document with unreadable text from DEP Box 22, folder GCMS X 11/23/01 A 11/29/01.
Filed in the same folder
NYC-WTC_000034719
Gas chromatography-mass spectrometry laboratory analytical data sheet with sample identification numbers, volumetric measurements, drip rates, and final analysis values from…
Filed in the same folder
NYC-WTC_000034722
Gas chromatography-mass spectrometry reference report listing concentrations of volatile organic compounds for sample AD28593.
Filed in the same folder
NYC-WTC_000034727
Calibration results for gas chromatography-mass spectrometry analysis showing detector responses for standard compounds.
Filed in the same folder
NYC-WTC_000034731
Instrument blank report confirming absence of target analytes in the analytical system prior to sample testing.
Filed in the same folder