GCMS re-analysis comments, sample AD29232, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1001\29232.D Vial: 16 Acq On : 11 Dec 2001 1:22 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.34 2.14 ug/1 589694 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Butanol, 3,3* -oxybis- 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 50 4 1-Propanol, 2-(2-hyd c propoxy) - 134 C6H14O3 000106-62-7 45 Abundance Scan 686 (11.339 mln): 29232.D (-) m/z 59.00 10 .00% 59 5000 45 103 73

39 ! 85 91 ... ...... 130.... 11.00 11.20 11.40 11.60 ‘ I 1 ‘ । . I | I 1 I . । . . .'I [ . . . Tit m/ z 44.95 miz-? 20 30 40 50 6070 80100 110 120 90 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 11.00 11.20 11.40 11.60 73 31 m/z 103.05 31.71 36.72% , 130 • i : ' i ■ ■ 1 ’It ••। •i 1TT ' I ‘ ‘ ‘ I ' ‘ ‘ I ' ' ' ‘ I 4 ' • • । • • ■ • । m । . miz-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 Abundance #12859. 2-Butanol, 3.3°-oxybis- 59 — ———— V 11.00 11.20 11.40 11.60 5000 31 m/z 73.00 27.64% 45 103

-PI •i■■■■l'1•'i1■■■i■••■i■■•■i■■■ ■ i' ■ • • i ■ ■ ■ ' i 134 • ■ ■ ■ i ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance " — • . ’ #9233: 2-Propanol, 1-(2-methoxypropoxy)- V . I I TI » » » » । » » i i । ) j I TF 11 TTT 59 11.00 11.20 11.40 11.60 m/z 41.05 22.37% 5000

m/z~> 31 ______ I ‘ I ' ‘ 20 ml 45 ‘ 1U' 1 1 1 11 1 I ‘ 30 40 50 60 70 80 90 100 110 120 130 140 .1A n-1 Th TT । »T» । t । TI TTdnnnd 11.00 11.20 11.40 11.60

29232.D GCMS1126.M Fri Dec 14 16:11:16 2001 Page 2

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