Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
NYC-WTC_000036151–000036161Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1001\29231.D Vial: 24 Acq On : 11 Dec 2001 11:06 am Operator: 209 GALOS Sample : gc/ms scan 12/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 1 R.T. • EstConc Area Relative to ISTD R.T.
11.42 2.19 ug/1 619361 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(/-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Butanol, 3,3/-oxybis- 162 C8H18O3 054305-61-2 64 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 4 2-Propanol, /f-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 40 Abundance” C Scan 694 (11.418 min): 29231.D(-) m/z 59.05 100.00% 59
5000
-394453 — ■ TBT 85 45 73
i • • • • i ■ 103
— I I I I I I J / » 130 J I » I I TI T M I * 1 ' ■ 1 ‘ ' 1 I ‘‘prI 111 ‘ IT ‘ 11.00 1120 11.40 11.60 11.80 m/z 45.05 47.98%
X miz-> 20 30 40 50 60 70 180 90 100 110 120 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59
5000 103 TTT TI1181 11/1/8.8 11111115 45 11.00 11.20 11.40 11.60 11.80 73 31 m/z 103.05 36.40% •। TT ■ • TT * । > ——— ......... 0 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859. 2-Butanol. 3,3‘-oxybis-
m/z JA 59 r1 ■ 1 T1 TTT i' 1 TT T ’ 11.00 11.20 11.40 11.60 11.80 5000 31 45 103 । TIPP ।. -TT ■ i ■ ■ ■ ■ i 1 1 1 1 I 1 1 1 * I 1 ____________ 134 1TTTT II .-T-rr-p-r-n-j-T m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086:1-Propanol, 2-(2-h ) ypropox 59 11.00 11.20 11.40 11.60 11.80 m/z 5000 31 45 103
-PPPPP 4— । 11 . i’l—TT I | I 75 89 i' 4 : | » i » i j » i t i | » I TT j i I i I | ill i । I TTT | I 1 m/z—> 20 30 40 50 (60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80
29231.D GCMS1126.M Fri Dec 14 16:10:14 2001 Page 3
NYC-WTC_000036160
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NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034908
Repeat gas chromatography-mass spectrometry analysis of sample AD28596 after re-extraction, confirming bis(2-Ethylhexyl)phthalate at 0.36 ug/L with improved standard recovery of 89
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036103
Laboratory report noting GCMS scan results for sample AD29189 with di-n-butylphthalate detected and low pH.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036126
Laboratory report noting GCMS scan results for sample AD29287 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036114
Laboratory report noting GCMS scan results for sample AD29230 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036380
Laboratory report documenting GCMS analysis of sample AD29297 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
Filed in the same folder
NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
Filed in the same folder
NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder