GCMS analysis results for sample AD30251, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30251.D Vial: 8 Acq On : 27 Dec 2001 6:58 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Ethane, 1-ethoxy-1-methoxy- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

11.45 0.47 ug/1 151241 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethane, 1-ethoxy-l-methoxy- 104 C5H12O2 010471-14-4 64 2 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 56 3 Silane, trimethyl- 74 C3H10Si 000993-07-7 47 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance

5000 Scan 698 (11.453 min): 30251 .D (-)

39 — 4 45

1-51 59

ppll60 ■ Tr1f 85 73

I’niu 1,1 "p —r TImr m/z 45.05 103 .A m/z 59.05 100.00%

11.20 11.40 11.60 11.80 69.85%

N ‘ ‘ I • ■ 1 ■ i ■ • ■ ■ i • m/z-> 10 20 30 40 50 70 80 90 100 110 Abundance #1926: Ethane, 1 -ethoxy-1 -methoxy- 59 45

5000 ■— 49-IIII 73 89 11.20 11.40 11.60 11.80 27 m/z 41.05 40.12%

m/z-> Abundance

5000 11--- 11 * 10 20 30

31 40

45 50 60 1 I ' 1 11 1 ■ i'' ‘ i '

59 70 80 #6087; 2-Propanol. 1,1-oxybis- 'I ' r 11 1 •” ' > i । > 90 103 100 110 _MN m/z 11.20 11.40 11.60 11.80 ‘ 73.00 35.48%

.A 103 89 ■ ■ i ■ ■ ■ ■ i■ ■ ■ ■ i‘ 1 ■ ‘ i 1 1 ■ ' i • ' H TdnngnBmdgnangtu 72 I I I I « m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62564: Silane, trimethyl- ■ ■ ‘ ' f■ l I . I I I I . . . 59 11.20 11.40 11.60 11.80

miz-> 5000

■ • i 1 ■ 10 15 --- 20 30 31

40 50 60 73

— I —— I 70 80 90 100 110 m/z 103.05

A N 34.48%

11 i ' ■ ■ ’I****I**I*’ 11.20 11.40 11.60 11.80

30251.D GCMS1126.M Wed Jan 02 10:38:26 2002 Page 2

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