GCMS unknown compounds report, sample AD31501, Feb 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\ JANI80231501.D Vial: 11 Acq On : 19 Jan 2002 1:22 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C: \HPCHEM\1\METHODS\GCMS0103 :M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1,1’-oxybis- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.17 0.75 ug/1 197465 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1,1′-oxybi s- 134 C6H14O3 000110-98-5 50 2 Ethane, 1-ethoxy-1-methoxy- 104 C5H12O2 010471-14-4 45 3 1-Propanol,/-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 4 2 - Pent anone, 5-methoxy- 116 C6H12O2 017429-04-8 42 Abundance Scan 668 (11.174 mln): 31501 .D (-) 59 m/z 5905 " 45 5000 73 103 10.80 11.00 11.20 11.40 11.60

m/z-> mmPP -51-+ 39 84 89 Tmppppgpa] m/z , 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 45.05 Abundance #6087:2-Propanol, 1,1-oxybis- : 59 31 5000 45 1 i ■ ■ ■ ■ i T T 10.80 11.00 11.20 11.40 11.60 103 m/z 103.05 31.37%

m/z-> (4*3*444341 2’3331 _2 —ppt 1122271221111211110221101213302117181107717 mmgonunp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance 41928. Ethane. 1-ethoxv-1-mlery 59 45 ■ i 1 • ■ ■ I ■ • 1 1 » i ri । r fT j pr !I 10.80 11.00 11.20 11.40 11.60 5000 m/z 41.00 28.39% 73 89 27 _________________ J________ j__________________ TInuuu—muIuuuo"m010101000101191222233320 ; 103 —2231231190B31321923222132022222037171 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #6086:1-Propanoi, 2-(2-hydroxypropoxy)- Tr ■ i 1 ■ ' 1 i ■ ' ' ■ i 1 59 10.80 11.00 11.20 11.40 11.60 m/z 73.00. 27.27% 5000 31 45 103

75 89 TTTpn- TpH -j-l-rrrjTTTTp-rrTp-rTTpTrrp-r^^ miz-> ' ‘ I' ‘' • I'' ‘ ■ I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 10.80 11.00 11.20 11.40 11.60

31501.D GCMS0103.M Wed Feb 06 15:35:44 2002 Page 3

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