GCMS unknown compounds report, sample AD31501, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN1802\31501.D Vial: 11 Acq On : 19 Jan 2002 1:22 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.58 0.86 ug/1 225634 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone,/ 1,1,1-trichloro- 160 C3H3C130 000918-00-3 32 2 4-Cyclopentene-1,3-diol, cis- 100 C5H802 029783-26-4 25 3 4-Cyclopentene-1, 3-diol, trans- 100 C5H802 000694-47-3 9 4 Acetic acid, 2-propenyl ester 100 C5H802 000591-87-7 9 Abundance Scan 277 (7.584 min): 31501 .D (-) m/z 4 .00 100.00% 43

5000 Tann—nn—nmn—n/Bn/n 35 7.20 7.40 7.60 7.80 8.00 49 55 61 72 83.... 97,.... 112 119125 । >-[ 11 । । । i i 1111 .'ri । i 1 1118a . 114*4 . । i ... । rrr, ! . . ’ . . . . j i . . . j . • ■ ■ । • > m/z 124.8 8.80% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 .... ■..... W........ ■ I ‘ • I 1 ' 1 ’ 1 1 TrI.u I I I I I 7.20 7.40 7.60 7.80 8.00 15 m/z 6.99% I 35 49 85 97 117 125 IIPPTT ■ ' i 4 ■ ■ ■ i ■ ■ ■ ' i ■ ■ ' ' i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance *“881: 4-Cvclopenor 1 1 . .. 43 4™ 7.20 7.40 7.60 7.80 8.00 5000 53 81 m/z 46.95 5.98% : 71 ? .................. ........... ..... . ■ ■ i ■ • ■ • i ■ ‘ ■ i ■ • ■ • i ■ ■ ■ ■ i * • ‘' t • ■ ‘11 ‘ ■ * • i1 ■'' i ■ ■ ■ ■ i ■ mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1478:4-Cyclopentene-1,3-dioI. trans- i 43 7.20 7.40 7.60 * 7.80 ‘ 8.00 m/z 127.00 5.98% 57 5000 71 82

■ ■ i * ■ •' i ■ ■ • ■ i ■ ■ ■ ■ । ■ * > j > TTTHT’r 1 1 i ........... 100................................. . 1 A..... ,, m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.20 7.40 7.60 7.80 8.00

31501.D GCMS0103.M Wed Feb 06 15:35:39 2002 Page 2

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