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GCMS analysis results for sample AE00008, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00008 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050109–000050121

Folder label: “GCMS X 1/3/02 A 1/24/02

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Scanned page image, NYC-WTC_000050118
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\8.D Vial: 10 Acq On : 24 Jan 2002 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.18 0.27 ug/1 75561 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-l-methylet 148 C7H1603 020324-32-7 64 2 2-Propanol, 1,1'-oxybis- 134 C6H14O3 000110-98-5 56 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 4 Ethane, 1-ethoxy-l-methoxy­ 104 C5H12O2 _______ 010471-14-4 50 Abundance ' Scan 668 (11.178 min): 8.D (-) m/z 59.05 100.00% 59 45 I 5000- 73 103 M. m/z-> —l 30 40 111, 50 rmmPi IT 60 70 'T' 80 84 90 100 110 120 130 10.80 m/z 11.00 45.05 , 11.20 11.40 58.32% 11.60

Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy)- 59

5000 103 TF T" 45 10.80 11.00 11.20 11.40 11.60 73 31 m/z 103.05, 31.57% i । ._________ I__________ , j__________ ___________________________ b 130 ■ i ■ ■ > ■ i ■ ■ ■ ■ i ■ 1 l ■ ■ ' ■ i 1 1 ' ' I ■ • • ' i ' ‘ ' i ' 1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 Abundance #6087: 2-Propanol. 1,1-oxybis- 59 T I-" i 10.80 11.00 11.20 11.40 11.60 I 31 45 5000- m/z 73.00 29.24% 103 ■ 1 72 89 ' i ' ' ' ' i ' ' ■ ' i ■ ■ ■ ' i ■ ' 1 ' i ' 1 m/z—> 30 40 50 60 70 80 90 100 110 120 130 [Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 10.80 11.00 11.20 11.40 11.60 m/z 41.05 25.54% ....................... ..................... 5000- 31 45 103

ll 75 89 ■ • i ■ • ' * I ' • ■ ' I ' —I I1 1 1 ' I 1 1 1 1 I 1 1 ■ < । ■ • < > । • • ■ ■ । ■ ■ ■ ■ । ■ ■ > > । ■ ■ m/z-> 30 40 50 60 70 80 90 100 110 120 130 10.80 11.00 11.20 11.40 11.60

8.D GCMS0208.M Fri Feb 08 13:43:06 2002 Page 3

NYC-WTC_000050118

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NYC-WTC_000050118Source: NYC Law Department, mirrored locally

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