GCMS analysis results for sample AE00008, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN2402\8.D Vial: 10 Acq On : 24 Jan 2002 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* . Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.57 0.66 ug/1 185307 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 37 2 1H-Azonine, octahydro- 127 C8H17N 005661-71-2 9 3 4 -Penten- 2 -one 84 C5H80 013891-87-7 9 4 1-Fluorononane 146 C9H19F 000463-18-3 9 'Abundance Scan 275 (7.570 min): 8.D (-) m/ z 42.95 100.00% 43

5000

m/z-> Abundance

5000 « I 1 > ■ 10

15 I 20 ■ • ■ ■ । 30 37

35 ■ ■ • i' . I4,9 56 .6,3 । I I dpi । I I | I । i’r J I I i -i-1 40

43 50

49 TI 60 70

85 80 82

#12247: 2-Propanone, 1,1,1-trichloro-

97 Ai—i ) i i 11) ■■■.[>■ . . । . i l >'| > . 90 97 100 110 117 125 110 120

117 125 130

o7.20

7.20 7.40

7.40 m/z 124.95 7.60

7.60 7.80 8.39%

7.80 8.32% 8.00

8.00

m/z-> 10 20 30 40 50 60- 70 80 90 100 110 120 130 Abundance #64990: 1H-Azonine, octahydro- 30 56 Til' A' 7.20 7.40 7.60 7.80 8.00 70 5000 m/z 81.8 6.09% 127 42 84 96 ----- ' i ' ' ' ' i ■ ■ ' ' i ■ ■ ' ' i ■ ' ' 1 i ' ■ ' ' 1 112 m/z--> 10 20 30 40 50 60 70 80 !90 100 110 120 130 Abundance #555: 4-Penten-2-one 43 7.20 7.40 7.60 7.80 8.00 m/ z 82.8 5.66% 5000-

15

m/z-> .... 10 20 30 371 40 53 60 69 1 1 1 IPI-FI I | I I I I') I ... | . I 50 70 80 84 | 90 100 | | 110 | . I I , ( r 120 130 M A 7.20 7.40 7.60 7.80 8.00

8.D GCMS0208.M Fri Feb 08 13:43:02 2002 Page 2

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