GCMS analysis results for sample AE00005, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\5.D Vial: 12 Acq On : 24 Jan 2002 11:51 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.58 0.49 ug/1 149143 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 33 2 1-Fluorononane 146 C9H19F 000463-18-3 9 3 2-Acetyl/l,4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 7 4 Decane, 71 - fluoro-___________________ 160 C10H21F 000334-56-5 4 Abundance Scan 276 (7.576 min): 5.D (-) 1m/ z 43.05 100.00% ; 43

5000

37 -PPPP+ I I I ■ i . 11 I 49 11J1 00 61 II 82 88 97 1191251. I .11 7.20 7.40 7.60 7.80 14.65% 8.00 ■ ■ i ■ m/z 124.85 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- I 43

5000 7.20 7.40 7.60 7.80 8.00 15 m/ z 81.9,5 11.11% I •1• 35 i 49 85 97 117 125 I ■ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8922: 1-Flucrononane 43

7.20 7.40 7.60 7.80 8.00 5000 m/z 96.9.5 8.99% 56 27 70 84 97 33 | ■ ■ i ■ ■ i ' 1 ' ■ i • 1 ' ' i ' ■ ' ' i ' ' ' ' i ■ ' ' ■ i ' ' ' ’ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4332: 2-Acetyl-1,4,5,6-tetrahydropyridine 43 7.20 7.40 7.60 7.80 8.00 54 82 m/ z 82.85 7.09% 5000- 125

97 ----- ■ ■ i ■ • ’ ' i 1 H— —— 110....120I 1301 ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

5.D GCMS0208.M Fri Feb 08 13:40:01 2002 Page 2

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