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GCMS analysis results for sample AE00005, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00005 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050088–000050098

Folder label: “GCMS X 1/3/02 A 1/24/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\5.D Vial: 12 Acq On : 24 Jan 2002 11:51 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.43 3.27 ug/1 987059 1,4-Dichlorobenzene-d4 11.49

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9 'Abundance Scan 260 (7.429 min): 5.D (-) m/z 73.'0 3 100.00% 73

5000 43 I—PTT 7.00 7.20 7.40 7.60 7.80 38,1,1,1,-50,-55461 6711 1,78, . 103 m/z 43.05 34.14% miz->10 20 30 40 50 60 70 80 !90 100 110 Abundance #845: Silane, tetramethyl- 73

5000 i ■ ‘ ' i ■ 7.00 7.20 7.40 7.60 7.80 45 m/ z 41.0.0 11.86% 15 31 ,| 55 । 88 । i ' ■ ' ■ । ————————————— m/z-> 10 20 30 40 50 60 __ 70____ 80 90 100 110 'Abundance #292: N-Ethylformamide 30 73 ■ ' 0 . i-/ . . kin if — 7.00 7.20 7.40 7.60 7.80 5000 m/ z 45.0, 11.70% 44 58

i 1 15 i i -| -i—r-r i । ,1 1 i । 1 1 1 i ' ■ ■ ■ i ' ' ' 1 i ' ■ ' ' i ■ ' ' ■ i ' ' ■ ‘ i ' ‘ ■ i ' ' m/z-> 10 20 30 40__ 50____ 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- I 3b 7.00 7.20 7.40 7.60 7.80 m/z 71.00 6.63% 5000

——————— 15 41 , 55 70 87 TP-mTPP m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

5.D GCMS0208.M Fri Feb 08 13:39:57 2002 Page 1

NYC-WTC_000050095

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NYC-WTC_000050095Source: NYC Law Department, mirrored locally

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