GCMS analysis results for sample AD31404, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 602\31404.D Vial: 9 Acq On : 16 Jan 2002 7:27 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 3.75 ug/1 868766 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, hetramethyl- 88 C4H12Si 000075-76-3 47 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-methyl - 88 C4H802 000497-26-7 9 Abundance Scan 262 (7.450 min): 31404.D (-) m/z 73.00 100.00% 73

5000 43

103 7.20 7.40 7.60 7.80 38 I, | 50 55 .61 67, t 1, ■ • i ■ ■ 87 1**I1*I* । ■ । ■ i । । । ।‘ 1 1 । 1 ■ 1’21’1-1’1 rrratg"e m/z 43.00 32.31% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 aP111 7.20 7.40 7.60 7.80 45 m/z 41.05 11.08% 1 I5 ,1 S-L———L—LTT . ■ 1 1 I1. ■ I ?■. .1'1 . । । । i 53 59 88 ■ i ■ ■ • ■ i ■ ' ■ • i ■ ■ ■ ■ i ' miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance *762 ' Sntangmnine 3-methy- 30 TfTTT T" 1 4 I IOmprit 7.20 7.40 7.60 7.80 5000 m/z 45.00 11.07%

15 41 55 70 87 *4,1*****1**1**I4***I****/* m/z-> 10 20 30 40 50 60 70 80___ 90___ 100 110 Abundance

5000 30 #292: N-Ethylformamide 73 m/z TTQT • ■ ■ TTni FIIIt Era ■ 1* 7.20 7.40 7.60 7.80

44 58 15 ■ ■ 1’ ■■ i ■ • i • • • • i 1 1 ■ ■ i ■ ■ ■ ■ i ■ ‘ ■ • i ■ ■ ' ■ i ‘ —ITIPmme m/z-> 10 20 30 40 !50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31404.D GCMS0103.M Thu Feb 07 09:13:12 2002 Page 1

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